Cinnamaldehyde, (p-tolylsulfonyl)hydrazone

Base Information

• Chemical Name: Cinnamaldehyde, (p-tolylsulfonyl)hydrazone
• CAS No.: 7318-33-4
• Molecular Formula: C16H16N2O2S
• Molecular Weight: 300.381
• Hs Code.: 2935009090
• European Community (EC) Number: 657-070-6
• NSC Number: 131995
• Mol file: 7318-33-4.mol

Synonyms:Cinnamaldehyde, (p-tolylsulfonyl)hydrazone;Cinnamaldehyde tosylhydrazone;p-Toluenesulfonic acid, cinnamylidenehydrazide;Benzenesulfonic acid, 4-methyl-, (3-phenyl-2-propenylidene)hydrazide;7318-33-4;SCHEMBL8218311;SCHEMBL18173186;KTJCQVMWEPIPJX-WUSSVBECSA-N;NSC131995;STK434300;AKOS003240003;NSC-131995;SR-01000211665;SR-01000211665-1;Benzenesulfonic acid, (3-phenyl-2-propenylidene)hydrazide;4-methyl-N'-[(1E,2E)-3-phenylprop-2-en-1-ylidene]benzenesulfonohydrazide;4-Methyl-N'-[(E,2E)-3-phenyl-2-propenylidene]benzenesulfonohydrazide;4-Methyl-N'-[(E,2E)-3-phenyl-2-propenylidene]benzenesulfonohydrazide #

Chemical Property of Cinnamaldehyde, (p-tolylsulfonyl)hydrazone

Chemical Property:

• Boiling Point: 470.6°Cat760mmHg
• Flash Point: 238.4°C
• PSA: 66.91000
• Density: 1.14g/cm³
• LogP: 4.44420
• XLogP3: 3.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 300.09324893
• Heavy Atom Count: 21
• Complexity: 451

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)S(=O)(=O)NN=CC=CC2=CC=CC=C2
• Isomeric SMILES: CC1=CC=C(C=C1)S(=O)(=O)N/N=C/C=C/C2=CC=CC=C2

Technology Process of Cinnamaldehyde, (p-tolylsulfonyl)hydrazone

There total 4 articles about Cinnamaldehyde, (p-tolylsulfonyl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

(E)-3-phenylpropenal (14371-10-9) + toluene-4-sulfonamide (70-55-3) → 4-methyl-N′-((2E)-3-phenylallylidene)benzenesulfonohydrazide (7318-33-4,126801-51-2)

Guidance literature:

In ethanol; at 20 ℃; for 1h;

Reference yield: 50.0%

(E)-3-phenylpropenal (14371-10-9) + toluene-4-sulfonic acid hydrazide (1576-35-8) → 4-methyl-N′-((2E)-3-phenylallylidene)benzenesulfonohydrazide (7318-33-4,126801-51-2)

Guidance literature:

In methanol; at 60 ℃; for 0.0833333 - 1h;

DOI:10.1021/acs.joc.8b02623

Reference yield: 47.0%

3-phenyl-propenal (104-55-2) + toluene-4-sulfonic acid hydrazide (1576-35-8) → cinnamaldehyde tosylhydrazone (7318-33-4)

Guidance literature:

In methanol; at 20 ℃; for 2h;

DOI:10.1021/jo202598e

upstream raw materials:

(E)-3-phenylpropenal

toluene-4-sulfonic acid hydrazide

toluene-4-sulfonamide

3-phenyl-propenal

Downstream raw materials:

bis-((1Ξ,2E)-3-phenyl-allylidene)-hydrazine

(E)-1-methyl-4-((3-phenylprop-1-en-1-yl)sulfonyl)benzene

(E)-3-phenylpropenal

5-phenyl-1H-pyrazole

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