1,19-bis[4-(4'''-phenyl-2,2':6',2'':6'',2''':6''',2''''-quinquepyridin-4'-yl)phenyl]-1,4,7,10,13,16,19-heptaoxanonadecane

Base Information

Chemical Name:1,19-bis[4-(4'''-phenyl-2,2':6',2'':6'',2''':6''',2''''-quinquepyridin-4'-yl)phenyl]-1,4,7,10,13,16,19-heptaoxanonadecane
CAS No.:845781-59-1
Molecular Formula:C₈₆H₇₂N₁₀O₇
Molecular Weight:1357.58
Hs Code.:

Synonyms:1,19-bis[4-(4'''-phenyl-2,2':6',2'':6'',2''':6''',2''''-quinquepyridin-4'-yl)phenyl]-1,4,7,10,13,16,19-heptaoxanonadecane

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Chemical Property of 1,19-bis[4-(4'''-phenyl-2,2':6',2'':6'',2''':6''',2''''-quinquepyridin-4'-yl)phenyl]-1,4,7,10,13,16,19-heptaoxanonadecane

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Technology Process of 1,19-bis[4-(4'''-phenyl-2,2':6',2'':6'',2''':6''',2''''-quinquepyridin-4'-yl)phenyl]-1,4,7,10,13,16,19-heptaoxanonadecane

There total 1 articles about 1,19-bis[4-(4'''-phenyl-2,2':6',2'':6'',2''':6''',2''''-quinquepyridin-4'-yl)phenyl]-1,4,7,10,13,16,19-heptaoxanonadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 845781-58-0
4'-(4-hydroxyphenyl)-4'''-phenyl-2,2':6',2'':6'',2''':6''',2''''-quinquepyridine

: 42749-27-9
hexa(ethyleneglycol) ditosylate

: 845781-59-1
1,19-bis[4-(4'''-phenyl-2,2':6',2'':6'',2''':6''',2''''-quinquepyridin-4'-yl)phenyl]-1,4,7,10,13,16,19-heptaoxanonadecane

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 20h;
DOI:10.1039/b500209e

Reference yield: 74.0%

: 845781-59-1
1,19-bis[4-(4'''-phenyl-2,2':6',2'':6'',2''':6''',2''''-quinquepyridin-4'-yl)phenyl]-1,4,7,10,13,16,19-heptaoxanonadecane

: ammonium hexafluorophosphate

: 6046-93-1
copper(II) acetate monohydrate

: [Cu₂(1,19-bis[4-(4'''-phenyl-2,2':6',2'':6'',2''':6''',2''''-quinquepyridin-4'-yl)phenyl]-1,4,7,10,13,16,19-heptaoxanonadecane)][PF₆]3

Guidance literature:: In methanol; oligopyridine ligand and Cu acetate mixed in MeOH, pptn. by addn. of NH4PF6; ppt. washed with ice cold MeOH, H2O and Et2O; elem. anal.;
DOI:10.1016/j.inoche.2004.08.010