N-(4-bromo-benzyl)-N-(2,2-dimethoxy-ethyl)-4-methyl-benzenesulfonamide

Base Information

Chemical Name:N-(4-bromo-benzyl)-N-(2,2-dimethoxy-ethyl)-4-methyl-benzenesulfonamide
CAS No.:1036378-91-2
Molecular Formula:C₁₈H₂₂BrNO₄S
Molecular Weight:428.347
Hs Code.:

Synonyms:N-(4-bromo-benzyl)-N-(2,2-dimethoxy-ethyl)-4-methyl-benzenesulfonamide

Suppliers and Price of N-(4-bromo-benzyl)-N-(2,2-dimethoxy-ethyl)-4-methyl-benzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of N-(4-bromo-benzyl)-N-(2,2-dimethoxy-ethyl)-4-methyl-benzenesulfonamide

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-(4-bromo-benzyl)-N-(2,2-dimethoxy-ethyl)-4-methyl-benzenesulfonamide

There total 2 articles about N-(4-bromo-benzyl)-N-(2,2-dimethoxy-ethyl)-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1036378-89-8
2-(4-bromobenzylamino)acetaldehyde dimethyl aceta

: 1036378-91-2
N-(4-bromo-benzyl)-N-(2,2-dimethoxy-ethyl)-4-methyl-benzenesulfonamide

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃; for 3h;

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 1036378-91-2
N-(4-bromo-benzyl)-N-(2,2-dimethoxy-ethyl)-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tris(acetoxy)borohydride / methanol / 0 - 20 °C

2: triethylamine / methanol / 5 h / 0 - 20 °C

With sodium tris(acetoxy)borohydride; triethylamine; In methanol;
DOI:10.1016/j.cclet.2019.09.023

Reference yield:

: 1036378-91-2
N-(4-bromo-benzyl)-N-(2,2-dimethoxy-ethyl)-4-methyl-benzenesulfonamide

: 34784-05-9
6-bromo-isoquinoline

Guidance literature:: N-(4-bromo-benzyl)-N-(2,2-dimethoxy-ethyl)-4-methyl-benzenesulfonamide; With aluminum (III) chloride; In dichloromethane; at 20 ℃;

With sodium hydroxide; water; In dichloromethane; at 0 ℃;