C₂₁H₂₃NO₅S

Base Information

Chemical Name:C₂₁H₂₃NO₅S
CAS No.:1360464-28-3
Molecular Formula:C₂₁H₂₃NO₅S
Molecular Weight:401.483
Hs Code.:

C<sub>21</sub>H<sub>23</sub>NO<sub>5</sub>S

Synonyms:C₂₁H₂₃NO₅S

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Chemical Property of C₂₁H₂₃NO₅S

Chemical Property:

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Technology Process of C₂₁H₂₃NO₅S

There total 8 articles about C₂₁H₂₃NO₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1360464-24-9
C₂₃H₂₇NO₆S

: 1360464-28-3
C₂₁H₂₃NO₅S

Guidance literature:: With hydrogenchloride; In acetone; Reflux;
DOI:10.1016/j.bmcl.2011.12.057

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 1360464-28-3
C₂₁H₂₃NO₅S

Guidance literature:: Multi-step reaction with 10 steps

1: sodium hydride / tetrahydrofuran / Reflux

2: ytterbium(III) triflate / benzene / Reflux

3: sodium tris(acetoxy)borohydride; acetic acid / acetonitrile

4: sodium t-butanolate / tetrahydrofuran

5: lithium aluminium tetrahydride / diethyl ether

6: 20% palladium hydroxide on charcoal; hydrogen / methanol

7: potassium carbonate / dichloromethane

8: tributylphosphine / acetonitrile

9: 3-chloro-benzenecarboperoxoic acid / dichloromethane

10: hydrogenchloride / acetone / Reflux

With hydrogenchloride; lithium aluminium tetrahydride; tributylphosphine; 20% palladium hydroxide on charcoal; hydrogen; sodium tris(acetoxy)borohydride; sodium hydride; potassium carbonate; acetic acid; 3-chloro-benzenecarboperoxoic acid; sodium t-butanolate; ytterbium(III) triflate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetone; acetonitrile; benzene;
DOI:10.1016/j.bmcl.2011.12.057

Reference yield:

: 813445-20-4
(7R,8R)-8-((R)-1-phenyl-ethylamino)-1,4-dioxa-spiro[4.5]decane-7-carboxylic acid ethyl ester

: 1360464-28-3
C₂₁H₂₃NO₅S

Guidance literature:: Multi-step reaction with 6 steps

1: lithium aluminium tetrahydride / diethyl ether

2: 20% palladium hydroxide on charcoal; hydrogen / methanol

3: potassium carbonate / dichloromethane

4: tributylphosphine / acetonitrile

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane

6: hydrogenchloride / acetone / Reflux

With hydrogenchloride; lithium aluminium tetrahydride; tributylphosphine; 20% palladium hydroxide on charcoal; hydrogen; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In methanol; diethyl ether; dichloromethane; acetone; acetonitrile;
DOI:10.1016/j.bmcl.2011.12.057