benzyl 4-carbamoyl-3'-formyl-5'-nitrobiphenyl-2-carboxylate

Base Information

Chemical Name:benzyl 4-carbamoyl-3'-formyl-5'-nitrobiphenyl-2-carboxylate
CAS No.:762254-56-8
Molecular Formula:C₂₂H₁₆N₂O₆
Molecular Weight:404.379
Hs Code.:

Synonyms:benzyl 4-carbamoyl-3'-formyl-5'-nitrobiphenyl-2-carboxylate

Suppliers and Price of benzyl 4-carbamoyl-3'-formyl-5'-nitrobiphenyl-2-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl 4-carbamoyl-3'-formyl-5'-nitrobiphenyl-2-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl 4-carbamoyl-3'-formyl-5'-nitrobiphenyl-2-carboxylate

There total 6 articles about benzyl 4-carbamoyl-3'-formyl-5'-nitrobiphenyl-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 762254-54-6
C₂₂H₁₈N₂O₆

: 762254-56-8
benzyl 4-carbamoyl-3'-formyl-5'-nitrobiphenyl-2-carboxylate

Guidance literature:: With manganese(IV) oxide; In benzene; for 20h; Heating / reflux;

Reference yield:

: 762254-26-2
benzyl 2-bromo-5-cyanobenzoate

: 762254-56-8
benzyl 4-carbamoyl-3'-formyl-5'-nitrobiphenyl-2-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate; dihydrogen peroxide / N,N-dimethyl-formamide / 12 h / 0 - 20 °C / Inert atmosphere

2.1: potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere

3.1: triethylamine; isobutyl chloroformate / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere

3.2: 1.5 h / 20 °C / Inert atmosphere

4.1: manganese(IV) oxide / benzene / 20 h / Reflux; Inert atmosphere

With manganese(IV) oxide; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dihydrogen peroxide; potassium carbonate; triethylamine; isobutyl chloroformate; In tetrahydrofuran; N,N-dimethyl-formamide; benzene; 2.1: |Suzuki Coupling;
DOI:10.1021/jm401670x

Reference yield:

: 25252-00-0
2-bromo-5-iodobenzoic acid

: 762254-56-8
benzyl 4-carbamoyl-3'-formyl-5'-nitrobiphenyl-2-carboxylate

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 4 h / 90 °C / Inert atmosphere

3.1: potassium carbonate; dihydrogen peroxide / N,N-dimethyl-formamide / 12 h / 0 - 20 °C / Inert atmosphere

4.1: potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere

5.1: triethylamine; isobutyl chloroformate / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere

5.2: 1.5 h / 20 °C / Inert atmosphere

6.1: manganese(IV) oxide / benzene / 20 h / Reflux; Inert atmosphere

With manganese(IV) oxide; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dihydrogen peroxide; potassium carbonate; potassium hydrogencarbonate; triethylamine; isobutyl chloroformate; In tetrahydrofuran; N,N-dimethyl-formamide; benzene; 4.1: |Suzuki Coupling;
DOI:10.1021/jm401670x