2-pentylcyclohexane

Base Information

• Chemical Name: 2-pentylcyclohexane
• CAS No.: 61208-94-4
• Molecular Formula: C₁₁H₂₂
• Molecular Weight: 154.296
• Mol file: 61208-94-4.mol

Synonyms:2-pentylcyclohexane

Chemical Property of 2-pentylcyclohexane

Chemical Property:

Purity/Quality:

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Technology Process of 2-pentylcyclohexane

There total 6 articles about 2-pentylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohex-1-en-1-yl trifluoromethane sulfonate (28075-50-5) + pentane (109-66-0,8031-35-4,9078-70-0) → 3-pentylcyclohexane (26321-98-2) + n-pentylcyclohexane (4292-92-6) + 2-pentylcyclohexane (61208-94-4)

Guidance literature:

With triethylsilane; triphenylmethyl closo-1,2,3,4,5,6,7,8,9,10,11-undecachloroundecacarborate; at 30 ℃; for 1.5h; Overall yield = 68 %Chromat.; regioselective reaction; Inert atmosphere;

DOI:10.1126/science.aat5440

Reference yield:

1-(furan-2-yl)-4-hydroxypent-1-en-3-one → 3-pentylcyclohexane (26321-98-2) + propylcyclohexane (1678-92-8) + 2-pentylcyclohexane (61208-94-4) + 2-methylbutyl-cyclohexane (54105-77-0)

Guidance literature:

With 5%-palladium/activated carbon; hydrogen; In water; at 163.84 ℃; for 8h; under 22502.3 Torr; High pressure;

DOI:10.1039/c5gc02414e

Reference yield:

pentyl chloroformate (638-41-5) + cyclohexene (110-83-8) → 3-pentylcyclohexane (26321-98-2) + 2-pentylcyclohexane (61208-94-4)

Guidance literature:

With triethylsilane; triethyl aluminum sesquichloride; In dichloromethane; at -15 - 20 ℃; for 2h; Title compound not separated from byproducts;

DOI:10.1021/ja048904y

upstream raw materials:

pentyl chloroformate

cyclohexene

1-ethylpropyl carbonochloridate

cyclohex-1-en-1-yl trifluoromethane sulfonate