N-[[1-{3-(1,2,3-triazol-1-yl)propyl}piperidin-4-yl]methyl]-4-amino-5-chloro-2-methoxybenzamide

Base Information

Chemical Name:N-[[1-{3-(1,2,3-triazol-1-yl)propyl}piperidin-4-yl]methyl]-4-amino-5-chloro-2-methoxybenzamide
CAS No.:1342815-16-0
Molecular Formula:C₁₉H₂₇ClN₆O₂
Molecular Weight:406.915
Hs Code.:

Synonyms:N-[[1-{3-(1,2,3-triazol-1-yl)propyl}piperidin-4-yl]methyl]-4-amino-5-chloro-2-methoxybenzamide

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Chemical Property of N-[[1-{3-(1,2,3-triazol-1-yl)propyl}piperidin-4-yl]methyl]-4-amino-5-chloro-2-methoxybenzamide

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Technology Process of N-[[1-{3-(1,2,3-triazol-1-yl)propyl}piperidin-4-yl]methyl]-4-amino-5-chloro-2-methoxybenzamide

There total 18 articles about N-[[1-{3-(1,2,3-triazol-1-yl)propyl}piperidin-4-yl]methyl]-4-amino-5-chloro-2-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 7206-70-4
4-amino-5-chloro-2-methoxybenzoic acid

: 1-[{3-(1H-1,2,3-triazol-1-yl)propyl}piperidin-4-yl]methanamine

: 1342815-16-0
N-[[1-{3-(1,2,3-triazol-1-yl)propyl}piperidin-4-yl]methyl]-4-amino-5-chloro-2-methoxybenzamide

Guidance literature:: 4-amino-5-chloro-2-methoxybenzoic acid; With 1,1'-carbonyldiimidazole; In acetonitrile; at 19 - 22 ℃; for 4h;

1-[{3-(1H-1,2,3-triazol-1-yl)propyl}piperidin-4-yl]methanamine; With triethylamine; In acetonitrile; for 21h; Reagent/catalyst; Solvent; Temperature; Reflux;

Reference yield: 100.0%

: 7206-70-4
4-amino-5-chloro-2-methoxybenzoic acid

: 1-[{3-(1H-1,2,3-triazol-1-yl)propyl}piperidin-4-yl]methanamine L-tartrate

: 1342815-16-0
N-[[1-{3-(1,2,3-triazol-1-yl)propyl}piperidin-4-yl]methyl]-4-amino-5-chloro-2-methoxybenzamide

Guidance literature:: 4-amino-5-chloro-2-methoxybenzoic acid; With 4-methyl-morpholine; isobutyl chloroformate; In dichloromethane; for 3h; Cooling;

1-[{3-(1H-1,2,3-triazol-1-yl)propyl}piperidin-4-yl]methanamine L-tartrate; With triethylamine; In dichloromethane; for 14h; Reagent/catalyst; Solvent; Temperature; Reflux;

Reference yield: 98.0%

: 7206-70-4
4-amino-5-chloro-2-methoxybenzoic acid

: 1-[{3-(1H-1,2,3-triazol-1-yl)propyl}piperidin-4-yl]methanamine hydrochloride

: 1342815-16-0
N-[[1-{3-(1,2,3-triazol-1-yl)propyl}piperidin-4-yl]methyl]-4-amino-5-chloro-2-methoxybenzamide

Guidance literature:: 4-amino-5-chloro-2-methoxybenzoic acid; With 4-methyl-morpholine; isobutyl chloroformate; In dichloromethane; for 3h; Cooling;

1-[{3-(1H-1,2,3-triazol-1-yl)propyl}piperidin-4-yl]methanamine hydrochloride; With triethylamine; In dichloromethane; for 4h; Reagent/catalyst; Solvent; Temperature; Reflux;