Technology Process of 2,5-diiodo-1,4-benzenedicarboxaldehyde
There total 4 articles about 2,5-diiodo-1,4-benzenedicarboxaldehyde which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine;
at 20 ℃;
for 2h;
Schlenk technique;
Inert atmosphere;
DOI:10.1021/jo401065b
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine / tetrahydrofuran / 20 °C / Schlenk technique; Inert atmosphere
2: iodine; periodic acid; acetic acid; sulfuric acid / water; tetrachloromethane / 15 h / Schlenk technique; Inert atmosphere; Reflux
3: sodium hydroxide / water; methanol / 12 h / Reflux
4: pyridinium chlorochromate / dichloromethane / 5 h / Reflux; Schlenk technique; Inert atmosphere
With
pyridine; sulfuric acid; iodine; acetic acid; periodic acid; pyridinium chlorochromate; sodium hydroxide;
In
tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; water;
DOI:10.1021/acs.joc.8b02557
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydroxide / water; methanol / 12 h / Reflux
2: pyridinium chlorochromate / dichloromethane / 5 h / Reflux; Schlenk technique; Inert atmosphere
With
pyridinium chlorochromate; sodium hydroxide;
In
methanol; dichloromethane; water;
DOI:10.1021/acs.joc.8b02557
