methyl 3α-amino-7α,12α-bis[(phenylaminocarbonyl)amino]-5β-cholan-24-oate

Base Information

Chemical Name:methyl 3α-amino-7α,12α-bis[(phenylaminocarbonyl)amino]-5β-cholan-24-oate
CAS No.:862202-69-5
Molecular Formula:C₃₉H₅₅N₅O₄
Molecular Weight:657.897
Hs Code.:

Synonyms:methyl 3α-amino-7α,12α-bis[(phenylaminocarbonyl)amino]-5β-cholan-24-oate

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Chemical Property of methyl 3α-amino-7α,12α-bis[(phenylaminocarbonyl)amino]-5β-cholan-24-oate

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Technology Process of methyl 3α-amino-7α,12α-bis[(phenylaminocarbonyl)amino]-5β-cholan-24-oate

There total 4 articles about methyl 3α-amino-7α,12α-bis[(phenylaminocarbonyl)amino]-5β-cholan-24-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 648928-64-7
methyl 3α-azido-7α,12α-bis-[(phenylaminocarbonyl)amino]-5β-cholan-24-oate

: 862202-69-5
methyl 3α-amino-7α,12α-bis[(phenylaminocarbonyl)amino]-5β-cholan-24-oate

Guidance literature:: With acetic acid; zinc; for 24h;
DOI:10.1016/j.tet.2010.06.069

Reference yield:

: C₅₇H₆₈N₅O₄P

: 862202-69-5
methyl 3α-amino-7α,12α-bis[(phenylaminocarbonyl)amino]-5β-cholan-24-oate

Guidance literature:: With water; In tetrahydrofuran; Heating;
DOI:10.1002/anie.200502330

Reference yield:

: 241808-92-4
methyl 3α-azido-7α,12α-di[N-(t-butyloxycarbonyl)amino]-5β-cholan-24-oate

: 862202-69-5
methyl 3α-amino-7α,12α-bis[(phenylaminocarbonyl)amino]-5β-cholan-24-oate

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / trifluoroacetic acid / CH₂Cl₂ / 3 h

2: 86 percent / DMAP; triethylamine / tetrahydrofuran / 24 h / 50 °C

3: tetrahydrofuran

4: 1.30 g / water / tetrahydrofuran / Heating

With dmap; water; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.200502330