(4S)-N-(p-methoxybenzyl)-2,2-dioxo-1,2,3-oxathiazolidinone-4-carboxylic acid

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Chemical Name:(4S)-N-(p-methoxybenzyl)-2,2-dioxo-1,2,3-oxathiazolidinone-4-carboxylic acid
CAS No.:415919-24-3
Molecular Formula:C₁₁H₁₃NO₆S
Molecular Weight:287.293
Hs Code.:

Synonyms:(4S)-N-(p-methoxybenzyl)-2,2-dioxo-1,2,3-oxathiazolidinone-4-carboxylic acid

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Chemical Property of (4S)-N-(p-methoxybenzyl)-2,2-dioxo-1,2,3-oxathiazolidinone-4-carboxylic acid

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Technology Process of (4S)-N-(p-methoxybenzyl)-2,2-dioxo-1,2,3-oxathiazolidinone-4-carboxylic acid

There total 4 articles about (4S)-N-(p-methoxybenzyl)-2,2-dioxo-1,2,3-oxathiazolidinone-4-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 328974-07-8
(4S)-N-(p-methoxybenzyl)-2,2-dioxo-1,2,3-oxathiazolidinone-4-carboxylic acid benzyl ester

: 415919-24-3
(4S)-N-(p-methoxybenzyl)-2,2-dioxo-1,2,3-oxathiazolidinone-4-carboxylic acid

Guidance literature:: With hydrogen; 10percent Pd/C; In ethyl acetate; for 3h; under 760.051 Torr;
DOI:10.1021/ja011932l

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 415919-24-3
(4S)-N-(p-methoxybenzyl)-2,2-dioxo-1,2,3-oxathiazolidinone-4-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 10.6 g / AcOH; NaBH₃CN / methanol / 12 h / 20 °C

2: SOCl₂; pyridine / CH₂Cl₂ / -78 - 20 °C

3: 8.3 g / aq. NaIO₄; RuCl₃ / acetonitrile / 0.25 h

4: 100 percent / H₂ / 10percent Pd/C / ethyl acetate / 3 h / 760.05 Torr

With pyridine; ruthenium trichloride; sodium periodate; thionyl chloride; hydrogen; sodium cyanoborohydride; acetic acid; 10percent Pd/C; In methanol; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1021/ja011932l

Reference yield:

: 328974-05-6
N-(p-methoxybenzyl)-L-serine benzyl ester

: 415919-24-3
(4S)-N-(p-methoxybenzyl)-2,2-dioxo-1,2,3-oxathiazolidinone-4-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂; pyridine / CH₂Cl₂ / -78 - 20 °C

2: 8.3 g / aq. NaIO₄; RuCl₃ / acetonitrile / 0.25 h

3: 100 percent / H₂ / 10percent Pd/C / ethyl acetate / 3 h / 760.05 Torr

With pyridine; ruthenium trichloride; sodium periodate; thionyl chloride; hydrogen; 10percent Pd/C; In dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1021/ja011932l