C₂₃H₂₄N₂O₃

Base Information

Chemical Name:C₂₃H₂₄N₂O₃
CAS No.:798563-46-9
Molecular Formula:C₂₃H₂₄N₂O₃
Molecular Weight:376.455
Hs Code.:

C<sub>23</sub>H<sub>24</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₃H₂₄N₂O₃

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Chemical Property of C₂₃H₂₄N₂O₃

Chemical Property:

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Technology Process of C₂₃H₂₄N₂O₃

There total 8 articles about C₂₃H₂₄N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 798563-45-8
1-(3-isopropoxybenzyl)-4-chloromethyl-6,7-dimethoxyisoquinoline

: 798563-46-9
C₂₃H₂₄N₂O₃

Guidance literature:: With sodium cyanide; In ethanol; water; for 2h; Heating / reflux;

Reference yield:

: 93-17-4
3,4-dimethoxyphenylacetonitrile

: 798563-46-9
C₂₃H₂₄N₂O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: ethanol; sodium / toluene / 2 h / 80 - 85 °C

1.2: 2 h / 80 °C

2.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol; water / 2844.39 Torr

3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 20 °C

4.1: phosphorus pentachloride / dichloromethane / 0 - 20 °C

5.1: sulfur / 0.33 h / 165 °C

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Heating / reflux

7.1: methanesulfonyl chloride; triethylamine / dichloromethane / 0.33 h / 0 °C

7.2: 20 °C

8.1: sodium cyanide / ethanol; water / 2 h / Heating / reflux

With hydrogenchloride; lithium aluminium tetrahydride; ethanol; phosphorus pentachloride; sodium cyanide; hydrogen; sodium; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; sulfur; methanesulfonyl chloride; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; water; toluene;

Reference yield:

: 36848-69-8
ethyl 2-cyano-2-(3,4-dimethoxyphenyl)acetate

: 798563-46-9
C₂₃H₂₄N₂O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol; water / 2844.39 Torr

2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 20 °C

3.1: phosphorus pentachloride / dichloromethane / 0 - 20 °C

4.1: sulfur / 0.33 h / 165 °C

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Heating / reflux

6.1: methanesulfonyl chloride; triethylamine / dichloromethane / 0.33 h / 0 °C

6.2: 20 °C

7.1: sodium cyanide / ethanol; water / 2 h / Heating / reflux

With hydrogenchloride; lithium aluminium tetrahydride; phosphorus pentachloride; sodium cyanide; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; sulfur; methanesulfonyl chloride; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; water;