5-ethyl-8-phenyl-3-(β-D-ribofuranosyl)-3H-imidazo[4,5-d][1,2,6]oxadiazepine

Base Information

Chemical Name:5-ethyl-8-phenyl-3-(β-D-ribofuranosyl)-3H-imidazo[4,5-d][1,2,6]oxadiazepine
CAS No.:1394921-40-4
Molecular Formula:C₁₈H₂₀N₄O₅
Molecular Weight:372.381
Hs Code.:

Synonyms:5-ethyl-8-phenyl-3-(β-D-ribofuranosyl)-3H-imidazo[4,5-d][1,2,6]oxadiazepine

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Chemical Property of 5-ethyl-8-phenyl-3-(β-D-ribofuranosyl)-3H-imidazo[4,5-d][1,2,6]oxadiazepine

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Technology Process of 5-ethyl-8-phenyl-3-(β-D-ribofuranosyl)-3H-imidazo[4,5-d][1,2,6]oxadiazepine

There total 6 articles about 5-ethyl-8-phenyl-3-(β-D-ribofuranosyl)-3H-imidazo[4,5-d][1,2,6]oxadiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1394921-31-3
5-ethyl-8-phenyl-3-[2,3,5-tri-O-(tert-butyldimethylsilyl)-β-D-ribofuranosyl]-3H-imidazo[4,5-d][1,2,6]oxadiazepine

: 1394921-40-4
5-ethyl-8-phenyl-3-(β-D-ribofuranosyl)-3H-imidazo[4,5-d][1,2,6]oxadiazepine

Guidance literature:: With ammonium fluoride; In methanol; for 5h; Reflux;
DOI:10.1039/c2cc33511e

Reference yield:

: 2',3',5'-tri-O-(tert-butyldimethylsilyl)-6-phenyl nebularine N-1 oxide

: 1394921-40-4
5-ethyl-8-phenyl-3-(β-D-ribofuranosyl)-3H-imidazo[4,5-d][1,2,6]oxadiazepine

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

2: tert.-butylhydroperoxide / tetrachloromethane / 1 h / Reflux

3: ammonium fluoride / methanol / 5 h / Reflux

With tert.-butylhydroperoxide; ammonium fluoride; In tetrahydrofuran; methanol; tetrachloromethane;
DOI:10.1039/c2cc33511e

Reference yield:

: C₃₅H₆₂N₄O₅Si₃

: 1394921-40-4
5-ethyl-8-phenyl-3-(β-D-ribofuranosyl)-3H-imidazo[4,5-d][1,2,6]oxadiazepine

Guidance literature:: Multi-step reaction with 2 steps

1: tert.-butylhydroperoxide / tetrachloromethane / 1 h / Reflux

2: ammonium fluoride / methanol / 5 h / Reflux

With tert.-butylhydroperoxide; ammonium fluoride; In methanol; tetrachloromethane;
DOI:10.1039/c2cc33511e