(1R,6S)-6-Methanesulfonylaminocarbonyl-cyclohex-3-enecarboxylic acid isopropyl ester

Base Information

Chemical Name:(1R,6S)-6-Methanesulfonylaminocarbonyl-cyclohex-3-enecarboxylic acid isopropyl ester
CAS No.:180790-20-9
Molecular Formula:C₁₂H₁₉NO₅S
Molecular Weight:289.353
Hs Code.:

Synonyms:(1R,6S)-6-Methanesulfonylaminocarbonyl-cyclohex-3-enecarboxylic acid isopropyl ester

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Chemical Property of (1R,6S)-6-Methanesulfonylaminocarbonyl-cyclohex-3-enecarboxylic acid isopropyl ester

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Technology Process of (1R,6S)-6-Methanesulfonylaminocarbonyl-cyclohex-3-enecarboxylic acid isopropyl ester

There total 2 articles about (1R,6S)-6-Methanesulfonylaminocarbonyl-cyclohex-3-enecarboxylic acid isopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1469-48-3,565227-54-5
cis-1,2,3,6-Tetrahydrophthalimide

: 180790-20-9
(1R,6S)-6-Methanesulfonylaminocarbonyl-cyclohex-3-enecarboxylic acid isopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Et₃N / 1.) MeCN, 0 degC, 10 min; 2.) MeCN, 2.5 h

2: 1.) (2-naphthyl)-substituted TADDOL / 1.) Et₂O, r.t., 3 h; 2.) THF, -30 degC, 21 d

With (2-naphthyl)-substituted TADDOL; triethylamine;
DOI:10.1002/hlca.19960790328

Reference yield:

: 546-68-9
titanium(IV)isopropoxide

: 180790-14-1
(3aR,7aS)-2-Methanesulfonyl-3a,4,7,7a-tetrahydro-isoindole-1,3-dione

: 180790-20-9
(1R,6S)-6-Methanesulfonylaminocarbonyl-cyclohex-3-enecarboxylic acid isopropyl ester

Guidance literature:: With (2-naphthyl)-substituted TADDOL; Yield given. Multistep reaction; 1.) Et₂O, r.t., 3 h; 2.) THF, -30 degC, 21 d;
DOI:10.1002/hlca.19960790328