ethyl 4-benzyloxy-6-[(2'-heptyl-1',3'-dioxolan-2'-yl)methyl]-2-hydroxybenzoate

Base Information

Chemical Name:ethyl 4-benzyloxy-6-[(2'-heptyl-1',3'-dioxolan-2'-yl)methyl]-2-hydroxybenzoate
CAS No.:184374-99-0
Molecular Formula:C₂₇H₃₆O₆
Molecular Weight:456.579
Hs Code.:

Synonyms:ethyl 4-benzyloxy-6-[(2'-heptyl-1',3'-dioxolan-2'-yl)methyl]-2-hydroxybenzoate

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Chemical Property of ethyl 4-benzyloxy-6-[(2'-heptyl-1',3'-dioxolan-2'-yl)methyl]-2-hydroxybenzoate

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Technology Process of ethyl 4-benzyloxy-6-[(2'-heptyl-1',3'-dioxolan-2'-yl)methyl]-2-hydroxybenzoate

There total 7 articles about ethyl 4-benzyloxy-6-[(2'-heptyl-1',3'-dioxolan-2'-yl)methyl]-2-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 100-39-0
benzyl bromide

: 184374-94-5
ethyl 6-[(2'-heptyl-1',3'-dioxolan-2'-yl)methyl]-2,4-dihydroxybenzoate

: 184374-99-0
ethyl 4-benzyloxy-6-[(2'-heptyl-1',3'-dioxolan-2'-yl)methyl]-2-hydroxybenzoate

Guidance literature:: With sodium hydrogencarbonate; In N,N-dimethyl-formamide; for 21h;
DOI:10.1071/ch9960917

Reference yield:

: 13195-66-9
ethyl 3-oxodecanoate

: 184374-99-0
ethyl 4-benzyloxy-6-[(2'-heptyl-1',3'-dioxolan-2'-yl)methyl]-2-hydroxybenzoate

Guidance literature:: Multi-step reaction with 7 steps

1: 82 percent / p-toluenesulfonic acid / toluene / 5 h / Heating

2: 90 percent / LiAlH₄ / diethyl ether / 4 h / Heating

3: 81 percent / pyridinium dichromate / CH₂Cl₂ / 22 h / Heating

4: 48 percent / toluene / 21 h / 50 °C

5: 1.) sodium, ethanol / 1.) r.t., 30 min, 2.) ethanol, reflux, 24 h

7: 19 percent / sodium hydrogen carbonate / dimethylformamide / 21 h

With lithium aluminium tetrahydride; dipyridinium dichromate; ethanol; sodium; sodium hydrogencarbonate; toluene-4-sulfonic acid; In diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1071/ch9960917

Reference yield:

: 161838-89-7
2-(2-hydroxyethyl)-2-heptyl-1,3-dioxolane

: 184374-99-0
ethyl 4-benzyloxy-6-[(2'-heptyl-1',3'-dioxolan-2'-yl)methyl]-2-hydroxybenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: 81 percent / pyridinium dichromate / CH₂Cl₂ / 22 h / Heating

2: 48 percent / toluene / 21 h / 50 °C

3: 1.) sodium, ethanol / 1.) r.t., 30 min, 2.) ethanol, reflux, 24 h

5: 19 percent / sodium hydrogen carbonate / dimethylformamide / 21 h

With dipyridinium dichromate; ethanol; sodium; sodium hydrogencarbonate; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1071/ch9960917