2-(4-methoxyphenethyl)quinoline

Base Information

Chemical Name:2-(4-methoxyphenethyl)quinoline
CAS No.:95742-49-7
Molecular Formula:C₁₈H₁₇NO
Molecular Weight:263.339
Hs Code.:

Synonyms:2-(4-methoxyphenethyl)quinoline

Suppliers and Price of 2-(4-methoxyphenethyl)quinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-methoxyphenethyl)quinoline

Chemical Property:

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Technology Process of 2-(4-methoxyphenethyl)quinoline

There total 8 articles about 2-(4-methoxyphenethyl)quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 91-63-4
2-methylquinoline

: 105-13-5
4-Methoxybenzyl alcohol

: 95742-49-7
2-(4-methoxyphenethyl)quinoline

Guidance literature:: With 1,10-Phenanthroline; potassium tert-butylate; nickel dibromide; In toluene; at 140 ℃; for 24h; chemoselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1039/c8cc06370b

Reference yield: 34.0%

: 91-63-4
2-methylquinoline

: 105-13-5
4-Methoxybenzyl alcohol

: 95742-49-7
2-(4-methoxyphenethyl)quinoline

: Anisylidenchinaldin

Guidance literature:: With 1,10-Phenanthroline; potassium tert-butylate; iron(II) acetate; In 1,4-dioxane; at 140 ℃; for 10h; Inert atmosphere;
DOI:10.1039/d0cc01593h

Reference yield:

: 1780-19-4
1,2,3,4-tetrahydro-2-methylquinoline

: 95742-49-7
2-(4-methoxyphenethyl)quinoline

Guidance literature:: Multi-step reaction with 4 steps

1: nickel dibromide; potassium tert-butylate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 1,10-Phenanthroline; oxygen / tert-Amyl alcohol / 24 h / 95 °C

2: toluene-4-sulfonamide / toluene / 24 h / 120 °C

3: nickel(II) chloride hexahydrate; sodium tetrahydroborate; methanol / 4 h / 0 - 20 °C

4: nickel dibromide; potassium tert-butylate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 1,10-Phenanthroline; oxygen / tert-Amyl alcohol / 48 h / 95 °C

With methanol; sodium tetrahydroborate; 1,10-Phenanthroline; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; nickel(II) chloride hexahydrate; potassium tert-butylate; oxygen; toluene-4-sulfonamide; nickel dibromide; In tert-Amyl alcohol; toluene;
DOI:10.1021/acs.orglett.0c02271