cholesteryl retinoate

Base Information

Chemical Name:cholesteryl retinoate
CAS No.:16409-17-9
Molecular Formula:C₄₇H₇₂O₂
Molecular Weight:669.087
Hs Code.:

Synonyms:cholesteryl retinoate

Suppliers and Price of cholesteryl retinoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cholesteryl retinoate

Chemical Property:

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Technology Process of cholesteryl retinoate

There total 4 articles about cholesteryl retinoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 842127-17-7
5-benzenesulfonyl-3,7-dimethyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,6,8-trienoic acid 17-(1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

: 16409-17-9
cholesteryl retinoate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 20 ℃; for 4h;
DOI:10.1055/s-2004-834867

Reference yield: 85.0%

: 302-79-4
all-trans-retinoic-acid

: 57-88-5
cholesterol

: 16409-17-9
cholesteryl retinoate

Guidance literature:: With dicyclohexyl-carbodiimide; In diethyl ether; 1.) 0 deg C, 30 min, 2.) room temperature, 1 h;

Reference yield:

: 19041-16-8
(E)-4-bromo-3-methyl-2-butenoic acid

: 16409-17-9
cholesteryl retinoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl chloride / benzene

2.1: BuLi / tetrahydrofuran; hexane / 0.83 h / -78 °C

2.2: 74 percent / tetrahydrofuran; hexane / 0.5 h / -78 °C

3.1: BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

3.2: 69 percent / tetrahydrofuran; hexane / 1 h / -78 °C

4.1: 92 percent / DBU / tetrahydrofuran / 4 h / 20 °C

With n-butyllithium; oxalyl dichloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; hexane; benzene; 3.2: Julia olefination;
DOI:10.1055/s-2004-834867