(N-{4-[5-(phenanthren-2-yl)-3-(trifluoromethyl)-1H-pyrazol-1-yl]phenyl}sulfuric diamide)

Base Information

Chemical Name:(N-{4-[5-(phenanthren-2-yl)-3-(trifluoromethyl)-1H-pyrazol-1-yl]phenyl}sulfuric diamide)
CAS No.:1148047-04-4
Molecular Formula:C₂₄H₁₇F₃N₄O₂S
Molecular Weight:482.486
Hs Code.:

Synonyms:(N-{4-[5-(phenanthren-2-yl)-3-(trifluoromethyl)-1H-pyrazol-1-yl]phenyl}sulfuric diamide)

Suppliers and Price of (N-{4-[5-(phenanthren-2-yl)-3-(trifluoromethyl)-1H-pyrazol-1-yl]phenyl}sulfuric diamide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (N-{4-[5-(phenanthren-2-yl)-3-(trifluoromethyl)-1H-pyrazol-1-yl]phenyl}sulfuric diamide)

Chemical Property:

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Technology Process of (N-{4-[5-(phenanthren-2-yl)-3-(trifluoromethyl)-1H-pyrazol-1-yl]phenyl}sulfuric diamide)

There total 6 articles about (N-{4-[5-(phenanthren-2-yl)-3-(trifluoromethyl)-1H-pyrazol-1-yl]phenyl}sulfuric diamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₂₅F₃N₄O₄S

: 1148047-04-4
(N-{4-[5-(phenanthren-2-yl)-3-(trifluoromethyl)-1H-pyrazol-1-yl]phenyl}sulfuric diamide)

Guidance literature:: C₂₉H₂₅F₃N₄O₄S; With trifluoroacetic acid; In dichloromethane; for 1h;

With sodium hydrogencarbonate; In dichloromethane;
DOI:10.1016/j.bmc.2012.06.018

Reference yield:

: 882854-64-0
4-(5-phenanthren-2-yl-3-trifluoromethyl-pyrazol-1-yl)-phenylamine

: 1148047-04-4
(N-{4-[5-(phenanthren-2-yl)-3-(trifluoromethyl)-1H-pyrazol-1-yl]phenyl}sulfuric diamide)

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 1 h / 25 °C

2: trifluoroacetic acid / dichloromethane / 1 h

With triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmc.2012.06.018

Reference yield:

: 100-16-3
4-nitrophenylhydrazone

: 1148047-04-4
(N-{4-[5-(phenanthren-2-yl)-3-(trifluoromethyl)-1H-pyrazol-1-yl]phenyl}sulfuric diamide)

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / ethanol / Reflux

2: platinum(IV) oxide; hydrogen / ethanol

3: triethylamine / dichloromethane / 1 h / 25 °C

4: trifluoroacetic acid / dichloromethane / 1 h

With hydrogenchloride; platinum(IV) oxide; hydrogen; triethylamine; trifluoroacetic acid; In ethanol; dichloromethane;
DOI:10.1016/j.bmc.2012.06.018