4,4,4-TRIFLUORO-1-PHENANTHREN-2-YL-BUTANE-1,3-DIONE

Base Information

• Chemical Name: 4,4,4-TRIFLUORO-1-PHENANTHREN-2-YL-BUTANE-1,3-DIONE
• CAS No.: 15389-33-0
• Molecular Formula: C18H11F3O2
• Molecular Weight: 316.27400
• Hs Code.: 2914700090
• Mol file: 15389-33-0.mol

Synonyms:4,4,4-TRIFLUORO-1-PHENANTHREN-2-YL-BUTANE-1,3-DIONE;1,3-Butanedione,4,4,4-trifluoro-1-(2-phenanthrenyl);

Chemical Property of 4,4,4-TRIFLUORO-1-PHENANTHREN-2-YL-BUTANE-1,3-DIONE

Chemical Property:

• PSA: 34.14000
• LogP: 4.69720
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

4,4,4-Trifluoro-1-(phenanthren-2-yl)butane-1,3-dione 96% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,4,4-TRIFLUORO-1-PHENANTHREN-2-YL-BUTANE-1,3-DIONE

There total 1 articles about 4,4,4-TRIFLUORO-1-PHENANTHREN-2-YL-BUTANE-1,3-DIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

ethyl trifluoroacetate, (383-63-1) + 2-acetylphenanthrene (5960-69-0) → 4,4,4-Trifluoro-1-phenanthren-2-yl-butane-1,3-dione (15389-33-0)

Guidance literature:

With sodium hydride; In tetrahydrofuran;

Reference yield: 65.0%

4,4,4-Trifluoro-1-phenanthren-2-yl-butane-1,3-dione (15389-33-0) + 4-hydrazinobenzene-1-sulfonamide hydrochloride (17852-52-7,27918-19-0) → OSU-02067

Guidance literature:

In ethanol;

Reference yield:

4,4,4-Trifluoro-1-phenanthren-2-yl-butane-1,3-dione (15389-33-0) + 4-nitrophenylhydrazone (100-16-3) → C24H14F3N3O2 (1100051-52-2)

Guidance literature:

With hydrogenchloride; In ethanol; Reflux;

DOI:10.1016/j.bmc.2012.06.018

upstream raw materials:

ethyl trifluoroacetate,

2-acetylphenanthrene

Downstream raw materials:

2-amino-N-{4-[5-(2-phenanthrenyl)-3-(trifluoromethyl)-1H-pyrazol-1-yl]phenyl}acetamide

(N-{4-[5-(phenanthren-2-yl)-3-(trifluoromethyl)-1H-pyrazol-1-yl]phenyl}sulfuric diamide)

C₂₇H₂₁F₃N₄O

C₃₀H₂₈F₃N₅O