di-p-tolyl-p-styryltin di-t-butylphosphine

Base Information

Chemical Name:di-p-tolyl-p-styryltin di-t-butylphosphine
CAS No.:74347-43-6
Molecular Formula:C₃₀H₃₉PSn
Molecular Weight:549.323
Hs Code.:

Synonyms:di-p-tolyl-p-styryltin di-t-butylphosphine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di-p-tolyl-p-styryltin di-t-butylphosphine

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Technology Process of di-p-tolyl-p-styryltin di-t-butylphosphine

There total 1 articles about di-p-tolyl-p-styryltin di-t-butylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 74255-82-6
(p-styryl)di-p-tolyltin chloride

: 42491-34-9
di-tert-butyl(trimethylsilyl)phosphane

: 75-77-4
chloro-trimethyl-silane

: 74347-43-6
di-p-tolyl-p-styryltin di-t-butylphosphine

: tri-p-styryltin diphenylphosphine

: p-tolyl-di-p-styryltin diphenylphosphine

: tri-p-tolyltin diphenylphosphine

Guidance literature:: In diethyl ether; toluene; addn. of equimolar amts. of Me3SiP(t-Bu)2 in toluene to satd. soln. of (p-MePh)2(CH2CHPh)SnCl in ether, 1h, room temp., stirred, distn. under vac., under Ar; elem. anal., byproducts detected by NMR;
DOI:10.1016/S0022-328X(00)82878-8

Reference yield:

: 74347-43-6
di-p-tolyl-p-styryltin di-t-butylphosphine

: 13463-39-3,71564-36-8
tetracarbonyl nickel

: di-p-tolylstyryltin di-t-butylphosphinetricarbonylnickel

Guidance literature:: In pentane; byproducts: CO; addn. of Ni(CO)4 to soln. of Sn compd., -78°C, low press., warmed up to room temp., reaction monitored by measuring of formed CO, evapn.in vac., under Ar; recrystn. from pentane; elem. anal.;
DOI:10.1016/S0022-328X(00)82878-8