methyl 2-hydroxy-5-(4-methoxyphenyl)-3-methylenecyclohex-1-enecarboxylate

Base Information

Chemical Name:methyl 2-hydroxy-5-(4-methoxyphenyl)-3-methylenecyclohex-1-enecarboxylate
CAS No.:1258518-06-7
Molecular Formula:C₁₆H₁₈O₄
Molecular Weight:274.317
Hs Code.:

Synonyms:methyl 2-hydroxy-5-(4-methoxyphenyl)-3-methylenecyclohex-1-enecarboxylate

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Chemical Property of methyl 2-hydroxy-5-(4-methoxyphenyl)-3-methylenecyclohex-1-enecarboxylate

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Technology Process of methyl 2-hydroxy-5-(4-methoxyphenyl)-3-methylenecyclohex-1-enecarboxylate

There total 5 articles about methyl 2-hydroxy-5-(4-methoxyphenyl)-3-methylenecyclohex-1-enecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: methyl 2-(4-methoxyphenyl)-1-(2-((trimethylsilyl)methyl)acryloyl)cyclopropanecarboxylate

: 1258518-06-7
methyl 2-hydroxy-5-(4-methoxyphenyl)-3-methylenecyclohex-1-enecarboxylate

Guidance literature:: With indium(III) triflate; In dichloromethane; at 25 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1021/ol102497w

Reference yield: 46.0%

: 1258517-97-3
methyl 1-methacryloyl-2-(4-methoxyphenyl)cyclopropane-1-carboxylate

: 1258518-35-2
methyl 5-(4-methoxyphenyl)-3-methyl-2-oxoyclohex-3-enecarboxylate

: 1258518-06-7
methyl 2-hydroxy-5-(4-methoxyphenyl)-3-methylenecyclohex-1-enecarboxylate

Guidance literature:: With indium(III) triflate; In dichloromethane; at 25 ℃; for 0.666667h; Inert atmosphere;
DOI:10.1021/ol102497w

Reference yield:

: 1258517-97-3
methyl 1-methacryloyl-2-(4-methoxyphenyl)cyclopropane-1-carboxylate

: 762-72-1
allyl-trimethyl-silane

: 1258518-06-7
methyl 2-hydroxy-5-(4-methoxyphenyl)-3-methylenecyclohex-1-enecarboxylate

: methyl 5-allyl-4-hydroxy-4'-methoxy-5-methyl-1,2,5,6-tetrahydro-[1,1'-biphenyl]-3-carboxylate

: methyl 5-(4-methoxyphenyl)-2-((trimethylsilyl)methyl)-2,3,3a,4,5,6-hexahydrobenzofuran-7-carboxylate

: methyl 5-(4-methoxyphenyl)-2-((trimethylsilyl)methyl)-2,3,3a,4,5,6-hexahydrobenzofuran-7-carboxylate

Guidance literature:: With tin(IV) chloride; In dichloromethane; at -78 ℃; for 1.5h; Overall yield = 38 %; Overall yield = 0.054 g;
DOI:10.1021/ol503305r