Technology Process of C24H31F2N7O3S
There total 7 articles about C24H31F2N7O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium fluoride; sodium L-ascorbate;
copper(II) sulfate;
In
methanol; water;
at 40 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: trifluoroacetic acid; sodium nitrite / 0.5 h / 0 °C
1.2: 1.25 h
2.1: potassium fluoride; sodium L-ascorbate / copper(II) sulfate / water; methanol / 16 h / 40 °C
With
potassium fluoride; sodium L-ascorbate; trifluoroacetic acid; sodium nitrite;
copper(II) sulfate;
In
methanol; water;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium nitrate; sulfuric acid / 2 h / -10 - 20 °C
2.1: hydrogen / palladium 10% on activated carbon / methanol / 3 h / 10343.2 Torr / autoclave
3.1: pyridine / dichloromethane / 16 h / 20 °C
4.1: hydrogenchloride / ethanol; water / 2 h / 80 °C
5.1: trifluoroacetic acid; sodium nitrite / 0.5 h / 0 °C
5.2: 0.25 h
6.1: potassium fluoride; sodium L-ascorbate; copper(II) sulfate / water; methanol / 16 h / 40 °C
With
pyridine; hydrogenchloride; potassium fluoride; sulfuric acid; hydrogen; copper(II) sulfate; sodium L-ascorbate; potassium nitrate; trifluoroacetic acid; sodium nitrite;
palladium 10% on activated carbon;
In
methanol; ethanol; dichloromethane; water;