dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-4-O-(9-O-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-acetyl-β-D-glucopyranoside

Base Information

Chemical Name:dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-4-O-(9-O-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-acetyl-β-D-glucopyranoside
CAS No.:1198155-89-3
Molecular Formula:C₅₇H₆₉N₃O₁₆Si
Molecular Weight:1080.27
Hs Code.:

dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-4-O-(9-O-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-acetyl-β-D-glucopyranoside

Synonyms:dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-4-O-(9-O-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-acetyl-β-D-glucopyranoside

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Chemical Property of dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-4-O-(9-O-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-acetyl-β-D-glucopyranoside

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Technology Process of dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-4-O-(9-O-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-acetyl-β-D-glucopyranoside

There total 10 articles about dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-4-O-(9-O-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1198156-23-8
dimethylthexylsilyl O-(methyl 2-levulinoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-acetyl-β-D-glucopyranoside

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1198155-89-3
dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-4-O-(9-O-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-acetyl-β-D-glucopyranoside

Guidance literature:: With pyridine; dmap; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/ja907358k

Reference yield: 68.0%

: 1198155-89-3
dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-4-O-(9-O-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-acetyl-β-D-glucopyranoside

Guidance literature:

Reference yield: 27.0%

: 1577227-81-6
C₃₆H₃₄Cl₃NO₁₁

: dimethylthexylsilyl 6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

: 1198155-89-3
dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-4-O-(9-O-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-acetyl-β-D-glucopyranoside

Guidance literature:: C₃₆H₃₄Cl₃NO₁₁; dimethylthexylsilyl 6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranoside; In dichloromethane; toluene; at 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With trifluorormethanesulfonic acid; In tetrahydrofuran; toluene; at -30 ℃; Molecular sieve; Inert atmosphere;
DOI:10.1039/c3ob42312c