C₁₈H₁₇FN₆O₃S

Base Information

Chemical Name:C₁₈H₁₇FN₆O₃S
CAS No.:1338084-29-9
Molecular Formula:C₁₈H₁₇FN₆O₃S
Molecular Weight:416.436
Hs Code.:

C<sub>18</sub>H<sub>17</sub>FN<sub>6</sub>O<sub>3</sub>S

Synonyms:C₁₈H₁₇FN₆O₃S

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Chemical Property of C₁₈H₁₇FN₆O₃S

Chemical Property:

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Technology Process of C₁₈H₁₇FN₆O₃S

There total 5 articles about C₁₈H₁₇FN₆O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 6723-30-4
O-2-tetrahydro-2H-pyranhydroxylamine

: 1338084-08-4
C₁₃H₈FN₅O₂S

: 1338084-29-9
C₁₈H₁₇FN₆O₃S

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmcl.2011.08.022

Reference yield:

: 1338083-96-7
C₁₅H₁₂FN₅O₂S

: 1338084-29-9
C₁₈H₁₇FN₆O₃S

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol; sodium hydroxide / 20 °C / Reflux

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Inert atmosphere

With ethanol; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In dichloromethane;
DOI:10.1016/j.bmcl.2011.08.022

Reference yield:

: 459-38-1
(4-fluorobenzylidenehydrazinyl)thiocarboxamide

: 1338084-29-9
C₁₈H₁₇FN₆O₃S

Guidance literature:: Multi-step reaction with 4 steps

1.1: iron(III) chloride; sodium acetate / acetic acid / 0.5 h / 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 5 - 20 °C / Inert atmosphere

2.2: 5 °C / Inert atmosphere

3.1: ethanol; sodium hydroxide / 20 °C / Reflux

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Inert atmosphere

With iron(III) chloride; ethanol; sodium acetate; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In tetrahydrofuran; dichloromethane; acetic acid; mineral oil;
DOI:10.1016/j.bmcl.2011.08.022