2-(4-(2-(3,5-dimethylisoxazol-4-yl)-2-oxoethoxy)phenyl)-N-((2,4-dimethylphenyl)(phenyl)methyl)acetamide

Base Information

Chemical Name:2-(4-(2-(3,5-dimethylisoxazol-4-yl)-2-oxoethoxy)phenyl)-N-((2,4-dimethylphenyl)(phenyl)methyl)acetamide
CAS No.:1421838-41-6
Molecular Formula:C₃₀H₃₀N₂O₄
Molecular Weight:482.579
Hs Code.:

Synonyms:2-(4-(2-(3,5-dimethylisoxazol-4-yl)-2-oxoethoxy)phenyl)-N-((2,4-dimethylphenyl)(phenyl)methyl)acetamide

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Chemical Property of 2-(4-(2-(3,5-dimethylisoxazol-4-yl)-2-oxoethoxy)phenyl)-N-((2,4-dimethylphenyl)(phenyl)methyl)acetamide

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Technology Process of 2-(4-(2-(3,5-dimethylisoxazol-4-yl)-2-oxoethoxy)phenyl)-N-((2,4-dimethylphenyl)(phenyl)methyl)acetamide

There total 7 articles about 2-(4-(2-(3,5-dimethylisoxazol-4-yl)-2-oxoethoxy)phenyl)-N-((2,4-dimethylphenyl)(phenyl)methyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1402652-24-7
2-bromo-1-(3,5-dimethylisoxazol-4-yl)ethan-1-one

: 1421838-48-3
N-((2,4-dimethylphenyl)(phenyl)methyl)-2-(4-hydroxyphenyl)acetamide

: 1421838-41-6
2-(4-(2-(3,5-dimethylisoxazol-4-yl)-2-oxoethoxy)phenyl)-N-((2,4-dimethylphenyl)(phenyl)methyl)acetamide

Guidance literature:: With potassium carbonate; In acetonitrile; at 70 ℃; for 8h; Inert atmosphere;

Reference yield:

: 2510-36-3
3,5-dimethyl-4-isoxazolecarboxylic acid

: 1421838-41-6
2-(4-(2-(3,5-dimethylisoxazol-4-yl)-2-oxoethoxy)phenyl)-N-((2,4-dimethylphenyl)(phenyl)methyl)acetamide

Guidance literature:: Multi-step reaction with 7 steps

1: thionyl chloride / 70 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

3: Dess-Martin periodane / dichloromethane / 1.17 h / 0 - 20 °C

4: tetrahydrofuran; diethyl ether / 1.67 h / 0 - 20 °C

5: pyridinium chlorochromate / dichloromethane / 1 h / 0 - 20 °C

6: bromine; acetic acid / tetrachloromethane / 0.33 h / 48 °C

7: potassium carbonate / acetonitrile / 8 h / 70 °C / Inert atmosphere

With lithium aluminium tetrahydride; thionyl chloride; bromine; potassium carbonate; Dess-Martin periodane; acetic acid; pyridinium chlorochromate; In tetrahydrofuran; tetrachloromethane; diethyl ether; dichloromethane; acetonitrile;

Reference yield:

: 54593-26-9
3,5-dimethyl-1,2-oxazole-4-carbaldehyde

: 1421838-41-6
2-(4-(2-(3,5-dimethylisoxazol-4-yl)-2-oxoethoxy)phenyl)-N-((2,4-dimethylphenyl)(phenyl)methyl)acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran; diethyl ether / 1.67 h / 0 - 20 °C

2: pyridinium chlorochromate / dichloromethane / 1 h / 0 - 20 °C

3: bromine; acetic acid / tetrachloromethane / 0.33 h / 48 °C

4: potassium carbonate / acetonitrile / 8 h / 70 °C / Inert atmosphere

With bromine; potassium carbonate; acetic acid; pyridinium chlorochromate; In tetrahydrofuran; tetrachloromethane; diethyl ether; dichloromethane; acetonitrile;