trans-chlorocarbonylbis(triphenylphosphine)platinum(II) hexafluorophosphate

Base Information

Chemical Name:trans-chlorocarbonylbis(triphenylphosphine)platinum(II) hexafluorophosphate
CAS No.:85035-51-4
Molecular Formula:C₃₇H₃₀ClOP₂Pt*F₆P
Molecular Weight:928.089
Hs Code.:

Synonyms:trans-chlorocarbonylbis(triphenylphosphine)platinum(II) hexafluorophosphate

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Chemical Property of trans-chlorocarbonylbis(triphenylphosphine)platinum(II) hexafluorophosphate

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Technology Process of trans-chlorocarbonylbis(triphenylphosphine)platinum(II) hexafluorophosphate

There total 1 articles about trans-chlorocarbonylbis(triphenylphosphine)platinum(II) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 26042-63-7
silver(I) hexafluorophosphate

: 10199-34-5,14056-88-3,15604-36-1
bis(triphenylphosphine)platinum(II) dichloride

: 85035-51-4
trans-chlorocarbonylbis(triphenylphosphine)platinum(II) hexafluorophosphate

Guidance literature:: With carbon monoxide; In dichloromethane; acetonitrile; exclusion of moisture; soln. of AgPF6 in CH3CN added to soln. of Pt-compd. in CH2Cl2, stirred for 1 h; filtered (Celite), filtrate stirred under CO for 1.5 h, solvent stripped (vac.), recrystd. (CH2Cl2/Et2O); elem. anal.;

Reference yield: 86.3%

: 85035-51-4
trans-chlorocarbonylbis(triphenylphosphine)platinum(II) hexafluorophosphate

: 20524-03-2,22654-34-8
trans-chloro(ethoxycarbonyl)bis(triphenylphosphine)platinum(II)

Guidance literature:: With ethanol; In ethanol; educt and abs. ethanol stirred at room temp. for 23 h; ppt. collected on filter, washed with water, ethanol, and Et2O, dried, recystd. from CH2Cl2/hexane, washed with Et2O, dried in vac.; elem. anal.;
DOI:10.1016/0022-328X(83)80031-X

Reference yield: 59.0%

: 85035-51-4
trans-chlorocarbonylbis(triphenylphosphine)platinum(II) hexafluorophosphate

: 100-51-6,185532-71-2
benzyl alcohol

: 85024-90-4
trans-(benzoxycarbonyl)chlorobis(triphenylphosphine)platinum(II)

Guidance literature:: With sodium carbonate; In dichloromethane; benzyl alcohol; Pt complex and Na2CO3 dild. with CH2Cl2 and PhCH2OH, stirred for 24 h; concd., treated with Et2O and petroleum ether, cooled, crystals collected on filter, washed with water, benzyl alcohol, and Et2O, dried; elem. anal.;
DOI:10.1016/0022-328X(83)80031-X