(S)-2-benzyloxycarbonylamino-6-tert-butoxycarbonylaminohexanoic acid allyl ester

Base Information

Chemical Name:(S)-2-benzyloxycarbonylamino-6-tert-butoxycarbonylaminohexanoic acid allyl ester
CAS No.:918797-43-0
Molecular Formula:C₂₂H₃₂N₂O₆
Molecular Weight:420.506
Hs Code.:

Synonyms:(S)-2-benzyloxycarbonylamino-6-tert-butoxycarbonylaminohexanoic acid allyl ester

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Chemical Property of (S)-2-benzyloxycarbonylamino-6-tert-butoxycarbonylaminohexanoic acid allyl ester

Chemical Property:

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Technology Process of (S)-2-benzyloxycarbonylamino-6-tert-butoxycarbonylaminohexanoic acid allyl ester

There total 1 articles about (S)-2-benzyloxycarbonylamino-6-tert-butoxycarbonylaminohexanoic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: carboxybenzyl-L-lysine allyl ester

: 24424-99-5
di-tert-butyl dicarbonate

: 918797-43-0
(S)-2-benzyloxycarbonylamino-6-tert-butoxycarbonylaminohexanoic acid allyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1021/jm061033d

Reference yield:

: 918797-43-0
(S)-2-benzyloxycarbonylamino-6-tert-butoxycarbonylaminohexanoic acid allyl ester

: 918797-44-1
(S)-2-((S)-2-benzyloxycarbonylamino-4-methylpentanoylamino)-6-tert-butoxycarbonylaminohexanoic acid propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / methanol

2: N-methylmorpholine; 1-hydroxybenzotriazole; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium*PF₆ / dimethylformamide

With 4-methyl-morpholine; hydrogen; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm061033d

Reference yield:

: 918797-43-0
(S)-2-benzyloxycarbonylamino-6-tert-butoxycarbonylaminohexanoic acid allyl ester

: 4-{4-[1-(5-tert-butoxycarbonylamino-1-propoxycarbonyl-pentylcarbamoyl)-3-methyl-butylcarbamoyl]-phenoxy}-benzoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: H₂ / Pd/C / methanol

2: N-methylmorpholine; 1-hydroxybenzotriazole; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium*PF₆ / dimethylformamide

3: H₂ / Pd/C / methanol

4: 380 mg / N-methylmorpholine; 1-hydroxybenzotriazole; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium*PF₆ / dimethylformamide

5: H₂ / Pd/C / methanol

With 4-methyl-morpholine; hydrogen; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm061033d