(S)-2-((S)-2-benzyloxycarbonylamino-4-methylpentanoylamino)-6-tert-butoxycarbonylaminohexanoic acid propyl ester

Base Information

Chemical Name:(S)-2-((S)-2-benzyloxycarbonylamino-4-methylpentanoylamino)-6-tert-butoxycarbonylaminohexanoic acid propyl ester
CAS No.:918797-44-1
Molecular Formula:C₂₈H₄₅N₃O₇
Molecular Weight:535.681
Hs Code.:

Synonyms:(S)-2-((S)-2-benzyloxycarbonylamino-4-methylpentanoylamino)-6-tert-butoxycarbonylaminohexanoic acid propyl ester

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Chemical Property of (S)-2-((S)-2-benzyloxycarbonylamino-4-methylpentanoylamino)-6-tert-butoxycarbonylaminohexanoic acid propyl ester

Chemical Property:

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Technology Process of (S)-2-((S)-2-benzyloxycarbonylamino-4-methylpentanoylamino)-6-tert-butoxycarbonylaminohexanoic acid propyl ester

There total 4 articles about (S)-2-((S)-2-benzyloxycarbonylamino-4-methylpentanoylamino)-6-tert-butoxycarbonylaminohexanoic acid propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: carboxybenzyl-L-lysine allyl ester

: 918797-44-1
(S)-2-((S)-2-benzyloxycarbonylamino-4-methylpentanoylamino)-6-tert-butoxycarbonylaminohexanoic acid propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / 12 h / 20 °C

2: H₂ / Pd/C / methanol

3: N-methylmorpholine; 1-hydroxybenzotriazole; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium*PF₆ / dimethylformamide

With 4-methyl-morpholine; hydrogen; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm061033d

Reference yield:

: 918797-43-0
(S)-2-benzyloxycarbonylamino-6-tert-butoxycarbonylaminohexanoic acid allyl ester

: 918797-44-1
(S)-2-((S)-2-benzyloxycarbonylamino-4-methylpentanoylamino)-6-tert-butoxycarbonylaminohexanoic acid propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / methanol

2: N-methylmorpholine; 1-hydroxybenzotriazole; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium*PF₆ / dimethylformamide

With 4-methyl-morpholine; hydrogen; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm061033d

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 918797-44-1
(S)-2-((S)-2-benzyloxycarbonylamino-4-methylpentanoylamino)-6-tert-butoxycarbonylaminohexanoic acid propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / 12 h / 20 °C

2: H₂ / Pd/C / methanol

3: N-methylmorpholine; 1-hydroxybenzotriazole; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium*PF₆ / dimethylformamide

With 4-methyl-morpholine; hydrogen; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm061033d