N₁-p-methoxylphenyl-N₄-[1-butyl-2-carbonyl-2-(5-chloro-6-methoxynaphthalene-2-yl)]ethylpiperazine hydrochloride

Base Information

• Chemical Name: N₁-p-methoxylphenyl-N₄-[1-butyl-2-carbonyl-2-(5-chloro-6-methoxynaphthalene-2-yl)]ethylpiperazine hydrochloride
• CAS No.: 1221409-24-0
• Molecular Formula: C₂₈H₃₃ClN₂O₃*ClH
• Molecular Weight: 517.496

Synonyms:N₁-p-methoxylphenyl-N₄-[1-butyl-2-carbonyl-2-(5-chloro-6-methoxynaphthalene-2-yl)]ethylpiperazine hydrochloride

Chemical Property of N₁-p-methoxylphenyl-N₄-[1-butyl-2-carbonyl-2-(5-chloro-6-methoxynaphthalene-2-yl)]ethylpiperazine hydrochloride

Chemical Property:

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Technology Process of N₁-p-methoxylphenyl-N₄-[1-butyl-2-carbonyl-2-(5-chloro-6-methoxynaphthalene-2-yl)]ethylpiperazine hydrochloride

There total 4 articles about N₁-p-methoxylphenyl-N₄-[1-butyl-2-carbonyl-2-(5-chloro-6-methoxynaphthalene-2-yl)]ethylpiperazine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

4-(4-methoxyphenyl)piperazine (38212-30-5) + 2-bromo-1-(5-chloro-6-methoxynaphthalen-2-yl)-hexan-1-one (1221409-21-7) → N1-p-methoxylphenyl-N4-[1-butyl-2-carbonyl-2-(5-chloro-6-methoxynaphthalene-2-yl)]ethylpiperazine hydrochloride (1221409-24-0)

Guidance literature:

4-(4-methoxyphenyl)piperazine; 2-bromo-1-(5-chloro-6-methoxynaphthalen-2-yl)-hexan-1-one; With potassium carbonate; potassium iodide; In acetone; Reflux;

With hydrogenchloride; In ethanol;

Reference yield:

Hexanoyl chloride (142-61-0) → N1-p-methoxylphenyl-N4-[1-butyl-2-carbonyl-2-(5-chloro-6-methoxynaphthalene-2-yl)]ethylpiperazine hydrochloride (1221409-24-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: aluminum (III) chloride / dichloromethane / 1 h / 20 °C

1.2: 1 h / 10 - 20 °C

2.1: copper(ll) bromide / ethyl acetate; chloroform / 3 h / Reflux

3.1: potassium carbonate / potassium iodide / acetone / Reflux

With aluminum (III) chloride; potassium carbonate; copper(ll) bromide; potassium iodide; In dichloromethane; chloroform; ethyl acetate; acetone;

Reference yield:

1-chloro-2-methoxynaphthalene (13101-92-3) → N1-p-methoxylphenyl-N4-[1-butyl-2-carbonyl-2-(5-chloro-6-methoxynaphthalene-2-yl)]ethylpiperazine hydrochloride (1221409-24-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: aluminum (III) chloride / dichloromethane / 1 h / 20 °C

1.2: 1 h / 10 - 20 °C

2.1: copper(ll) bromide / ethyl acetate; chloroform / 3 h / Reflux

3.1: potassium carbonate / potassium iodide / acetone / Reflux

With aluminum (III) chloride; potassium carbonate; copper(ll) bromide; potassium iodide; In dichloromethane; chloroform; ethyl acetate; acetone;

upstream raw materials:

4-(4-methoxyphenyl)piperazine

2-bromo-1-(5-chloro-6-methoxynaphthalen-2-yl)-hexan-1-one

Hexanoyl chloride

1-chloro-2-methoxynaphthalene

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