α-cyanobenzyl diethyl phosphite

Base Information

Chemical Name:α-cyanobenzyl diethyl phosphite
CAS No.:83092-37-9
Molecular Formula:C₁₂H₁₆NO₃P
Molecular Weight:253.238
Hs Code.:

Synonyms:α-cyanobenzyl diethyl phosphite

Suppliers and Price of α-cyanobenzyl diethyl phosphite

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-cyanobenzyl diethyl phosphite

Chemical Property:

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Technology Process of α-cyanobenzyl diethyl phosphite

There total 2 articles about α-cyanobenzyl diethyl phosphite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 589-57-1
diethyl phosphorylchloridite

: 10020-96-9
(R)-Mandelonitrile

: 83092-37-9
α-cyanobenzyl diethyl phosphite

Guidance literature:: With pyridine; at -20 ℃;
DOI:10.1002/chem.200401290

Reference yield: 65.0%

: 33326-12-4
diethyl phosphorocyanidite

: 100-52-7
benzaldehyde

: 83092-37-9
α-cyanobenzyl diethyl phosphite

Guidance literature:: at 100 - 110 ℃; for 2h; sealed ampul, addition HCN or triethylamine accelerated the reaction;

Reference yield:

: 83092-37-9
α-cyanobenzyl diethyl phosphite

: 2549-14-6,1936-63-6
(R)-2-Amino-1-phenylethanol

Guidance literature:: Multi-step reaction with 2 steps

1: I₂ / tetrahydrofuran

2: 88 percent / LiAlH₄ / tetrahydrofuran / 4 h / 0 °C

With lithium aluminium tetrahydride; iodine; In tetrahydrofuran;
DOI:10.1002/chem.200401290