N-(benzyloxycarbonyl)ureido-N'-(tert-butyloxycarbonyl)-(S)-methylisothiourea

Base Information

Chemical Name:N-(benzyloxycarbonyl)ureido-N'-(tert-butyloxycarbonyl)-(S)-methylisothiourea
CAS No.:198416-20-5
Molecular Formula:C₁₆H₂₁N₃O₅S
Molecular Weight:367.426
Hs Code.:

Synonyms:N-(benzyloxycarbonyl)ureido-N'-(tert-butyloxycarbonyl)-(S)-methylisothiourea

Suppliers and Price of N-(benzyloxycarbonyl)ureido-N'-(tert-butyloxycarbonyl)-(S)-methylisothiourea

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(benzyloxycarbonyl)ureido-N'-(tert-butyloxycarbonyl)-(S)-methylisothiourea

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(benzyloxycarbonyl)ureido-N'-(tert-butyloxycarbonyl)-(S)-methylisothiourea

There total 1 articles about N-(benzyloxycarbonyl)ureido-N'-(tert-butyloxycarbonyl)-(S)-methylisothiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 69032-16-2
benzyloxycarbonyl isocyanate

: mono-(tert-butoxycarbonyl)-(S)-methylisothiourea

: 198416-20-5
N-(benzyloxycarbonyl)ureido-N'-(tert-butyloxycarbonyl)-(S)-methylisothiourea

Guidance literature:: In tetrahydrofuran; for 0.166667h; Ambient temperature;
DOI:10.1021/ja972670j

Reference yield: 30.0%

: 198416-20-5
N-(benzyloxycarbonyl)ureido-N'-(tert-butyloxycarbonyl)-(S)-methylisothiourea

: C₂₇H₃₄N₆O₆

: C₃₆H₄₁N₇O₉

: 198416-21-6
C₄₂H₅₁N₉O₁₁

Guidance literature:: With triethylamine; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1021/ja972670j

Reference yield:

: 198416-20-5
N-(benzyloxycarbonyl)ureido-N'-(tert-butyloxycarbonyl)-(S)-methylisothiourea

: C₂₂H₂₃N₅O₆

Guidance literature:: Multi-step reaction with 4 steps

1: CF₃COOH / 0.5 h / Ambient temperature

2: 41 percent / 1-(3-(dimethylamino)propyl)-3-ethylcarbodiimide hydrochloride, DMAP / CH₂Cl₂ / Ambient temperature

3: 82 percent / CF₃COOH, anisole / 5 h / Ambient temperature

4: 92 percent / Et₃N / dimethylformamide

With dmap; methoxybenzene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja972670j