7-<3-(9-acridinylamino)propyl>-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane

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Chemical Name:7-<3-(9-acridinylamino)propyl>-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane
CAS No.:117539-11-4
Molecular Formula:C₆₇H₈₂N₈O₁₂S₅
Molecular Weight:1351.76
Hs Code.:

Synonyms:7-<3-(9-acridinylamino)propyl>-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane

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Chemical Property of 7-<3-(9-acridinylamino)propyl>-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane

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Technology Process of 7-<3-(9-acridinylamino)propyl>-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane

There total 3 articles about 7-<3-(9-acridinylamino)propyl>-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1207-69-8
9-Chloroacridine

: 117539-10-3
7-(3-aminopropyl)-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane

: 117539-11-4
7-<3-(9-acridinylamino)propyl>-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane

Guidance literature:: With phenol; at 80 ℃; for 6h;
DOI:10.1021/ja00166a025

Reference yield:

: 107098-17-9
4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane

: 117539-11-4
7-<3-(9-acridinylamino)propyl>-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / tetrahydrofuran

2: 61 percent / B₂H₆ / tetrahydrofuran

3: 44 percent / phenol

With diborane; phenol; In tetrahydrofuran;
DOI:10.1039/c39880000596

Reference yield:

: 117539-09-0
3-[4,10,16,19,22-Pentakis-(toluene-4-sulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaaza-cyclotetracos-7-yl]-propionitrile

: 117539-11-4
7-<3-(9-acridinylamino)propyl>-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / B₂H₆ / tetrahydrofuran

2: 44 percent / phenol

With diborane; phenol; In tetrahydrofuran;
DOI:10.1039/c39880000596