2,3-dibromo-1-(2'-bromo-6'-bromomethyl-3',4'-dimethoxybenzyl)-4,5-dimethoxybenzene

Base Information

Chemical Name:2,3-dibromo-1-(2'-bromo-6'-bromomethyl-3',4'-dimethoxybenzyl)-4,5-dimethoxybenzene
CAS No.:1238891-84-3
Molecular Formula:C₁₈H₁₈Br₄O₄
Molecular Weight:617.955
Hs Code.:

Synonyms:2,3-dibromo-1-(2'-bromo-6'-bromomethyl-3',4'-dimethoxybenzyl)-4,5-dimethoxybenzene

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Chemical Property of 2,3-dibromo-1-(2'-bromo-6'-bromomethyl-3',4'-dimethoxybenzyl)-4,5-dimethoxybenzene

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Technology Process of 2,3-dibromo-1-(2'-bromo-6'-bromomethyl-3',4'-dimethoxybenzyl)-4,5-dimethoxybenzene

There total 8 articles about 2,3-dibromo-1-(2'-bromo-6'-bromomethyl-3',4'-dimethoxybenzyl)-4,5-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1026729-08-7
1-bromo-5-(bromomethyl)-2,3-dimethoxybenzene

: 4950-08-7
(2,3-dibromo-4,5-dimethoxyphenyl)methanol

: 1238891-84-3
2,3-dibromo-1-(2'-bromo-6'-bromomethyl-3',4'-dimethoxybenzyl)-4,5-dimethoxybenzene

Guidance literature:: With phosphorus pentoxide; phosphoric acid; at 80 ℃; for 0.5h; regioselective reaction;
DOI:10.1002/hlca.200900300

Reference yield:

: 1273542-60-1
2,3-dibromo-1-(2'-bromo-3',4'-dimethoxy-6'-methylbenzyl)-4,5-dimethoxy benzene

: 1238891-84-3
2,3-dibromo-1-(2'-bromo-6'-bromomethyl-3',4'-dimethoxybenzyl)-4,5-dimethoxybenzene

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; for 0.5h; Irradiation;
DOI:10.1016/j.ejmech.2013.03.037

Reference yield:

: 68278-85-3
3-bromo-4,5-dimethoxy-toluene

: 1238891-84-3
2,3-dibromo-1-(2'-bromo-6'-bromomethyl-3',4'-dimethoxybenzyl)-4,5-dimethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride / dichloromethane / 0.5 h / 0 - 20 °C

2: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 0.5 h / Irradiation

With aluminum (III) chloride; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; dichloromethane; 1: |Friedel-Crafts Alkylation;
DOI:10.1016/j.ejmech.2013.03.037