3(S)-imidazolecarbothioic acid 1,6-diphenyl-5(S)-tert-butoxycarbonylamino-2(S)-phenyl methoxycarbonylaminohexane ester

Base Information

Chemical Name:3(S)-imidazolecarbothioic acid 1,6-diphenyl-5(S)-tert-butoxycarbonylamino-2(S)-phenyl methoxycarbonylaminohexane ester
CAS No.:1448312-67-1
Molecular Formula:C₃₅H₄₀N₄O₅S
Molecular Weight:628.792
Hs Code.:

Synonyms:3(S)-imidazolecarbothioic acid 1,6-diphenyl-5(S)-tert-butoxycarbonylamino-2(S)-phenyl methoxycarbonylaminohexane ester

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Chemical Property of 3(S)-imidazolecarbothioic acid 1,6-diphenyl-5(S)-tert-butoxycarbonylamino-2(S)-phenyl methoxycarbonylaminohexane ester

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Technology Process of 3(S)-imidazolecarbothioic acid 1,6-diphenyl-5(S)-tert-butoxycarbonylamino-2(S)-phenyl methoxycarbonylaminohexane ester

There total 3 articles about 3(S)-imidazolecarbothioic acid 1,6-diphenyl-5(S)-tert-butoxycarbonylamino-2(S)-phenyl methoxycarbonylaminohexane ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 288-32-4
1H-imidazole

: 1448312-65-9
1,6-diphenyl-5(S)-tert-butoxycarbonylamino-3(S)-hydroxy-2(S)-phenylmethoxy-carbonylaminohexane

: 6160-65-2
1,1'-Thiocarbonyldiimidazole

: 1448312-67-1
3(S)-imidazolecarbothioic acid 1,6-diphenyl-5(S)-tert-butoxycarbonylamino-2(S)-phenyl methoxycarbonylaminohexane ester

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 48h;

Reference yield:

: 144163-85-9
(2S,3S,5S)-2-amino-3-hydroxy-5-(t-butyloxycarbonylamino)-1,6-diphenylhexane

: 1448312-67-1
3(S)-imidazolecarbothioic acid 1,6-diphenyl-5(S)-tert-butoxycarbonylamino-2(S)-phenyl methoxycarbonylaminohexane ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 0 - 20 °C

2: tetrahydrofuran / 48 h / 20 °C

With pyridine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1448312-67-1
3(S)-imidazolecarbothioic acid 1,6-diphenyl-5(S)-tert-butoxycarbonylamino-2(S)-phenyl methoxycarbonylaminohexane ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 0 - 20 °C

2: tetrahydrofuran / 48 h / 20 °C

With pyridine; In tetrahydrofuran; dichloromethane;