1,6-diphenyl-5(S)-tert-butoxycarbonylamino-3(S)-hydroxy-2(S)-phenylmethoxy-carbonylaminohexane

Base Information

Chemical Name:1,6-diphenyl-5(S)-tert-butoxycarbonylamino-3(S)-hydroxy-2(S)-phenylmethoxy-carbonylaminohexane
CAS No.:1448312-65-9
Molecular Formula:C₃₁H₃₈N₂O₅
Molecular Weight:518.653
Hs Code.:

Synonyms:1,6-diphenyl-5(S)-tert-butoxycarbonylamino-3(S)-hydroxy-2(S)-phenylmethoxy-carbonylaminohexane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,6-diphenyl-5(S)-tert-butoxycarbonylamino-3(S)-hydroxy-2(S)-phenylmethoxy-carbonylaminohexane

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Technology Process of 1,6-diphenyl-5(S)-tert-butoxycarbonylamino-3(S)-hydroxy-2(S)-phenylmethoxy-carbonylaminohexane

There total 1 articles about 1,6-diphenyl-5(S)-tert-butoxycarbonylamino-3(S)-hydroxy-2(S)-phenylmethoxy-carbonylaminohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 144163-85-9
(2S,3S,5S)-2-amino-3-hydroxy-5-(t-butyloxycarbonylamino)-1,6-diphenylhexane

: 1448312-65-9
1,6-diphenyl-5(S)-tert-butoxycarbonylamino-3(S)-hydroxy-2(S)-phenylmethoxy-carbonylaminohexane

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃;

Reference yield: 93.0%

: 288-32-4
1H-imidazole

: 1448312-65-9
1,6-diphenyl-5(S)-tert-butoxycarbonylamino-3(S)-hydroxy-2(S)-phenylmethoxy-carbonylaminohexane

: 6160-65-2
1,1'-Thiocarbonyldiimidazole

: 1448312-67-1
3(S)-imidazolecarbothioic acid 1,6-diphenyl-5(S)-tert-butoxycarbonylamino-2(S)-phenyl methoxycarbonylaminohexane ester

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 48h;

Reference yield: 74.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1448312-65-9
1,6-diphenyl-5(S)-tert-butoxycarbonylamino-3(S)-hydroxy-2(S)-phenylmethoxy-carbonylaminohexane

: 74-88-4
methyl iodide

: 1448312-66-0
3(S)-dithiocarbonic acid 1,6-diphenyl-5(S)-tert-butoxycarbonylamino-2(S)-phenylmethoxycarbonylaminohexane, methyl ester

Guidance literature:: 1,6-diphenyl-5(S)-tert-butoxycarbonylamino-3(S)-hydroxy-2(S)-phenylmethoxy-carbonylaminohexane; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.5h;

carbon disulfide; In tetrahydrofuran; mineral oil; for 1h;

methyl iodide; In tetrahydrofuran; mineral oil;