6-methyl-2-(2-hydroxyethyl)amino-8-(2-deoxy-3,5-di-O-p-toluoyl-β-D-ribofuranosyl)-O⁴-[2-(4-nitrophenyl)ethyl]-7(8H)-pteridinone

Base Information

• Chemical Name: 6-methyl-2-(2-hydroxyethyl)amino-8-(2-deoxy-3,5-di-O-p-toluoyl-β-D-ribofuranosyl)-O⁴-[2-(4-nitrophenyl)ethyl]-7(8H)-pteridinone
• CAS No.: 701285-29-2
• Molecular Formula: C₃₈H₃₈N₆O₁₀
• Molecular Weight: 738.754

Synonyms:6-methyl-2-(2-hydroxyethyl)amino-8-(2-deoxy-3,5-di-O-p-toluoyl-β-D-ribofuranosyl)-O⁴-[2-(4-nitrophenyl)ethyl]-7(8H)-pteridinone

Chemical Property of 6-methyl-2-(2-hydroxyethyl)amino-8-(2-deoxy-3,5-di-O-p-toluoyl-β-D-ribofuranosyl)-O⁴-[2-(4-nitrophenyl)ethyl]-7(8H)-pteridinone

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Technology Process of 6-methyl-2-(2-hydroxyethyl)amino-8-(2-deoxy-3,5-di-O-p-toluoyl-β-D-ribofuranosyl)-O⁴-[2-(4-nitrophenyl)ethyl]-7(8H)-pteridinone

There total 1 articles about 6-methyl-2-(2-hydroxyethyl)amino-8-(2-deoxy-3,5-di-O-p-toluoyl-β-D-ribofuranosyl)-O⁴-[2-(4-nitrophenyl)ethyl]-7(8H)-pteridinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

ethanolamine (141-43-5) + 8-(2-deoxy-3,5-di-O-toluoyl-β-D-ribofuranosyl)-6-methyl-2-methylsulfonyl-4-[2-(4-nitrophenyl)ethoxy]-8H-pteridin-7-one (174522-88-4) → 6-methyl-2-(2-hydroxyethyl)amino-8-(2-deoxy-3,5-di-O-p-toluoyl-β-D-ribofuranosyl)-O4-[2-(4-nitrophenyl)ethyl]-7(8H)-pteridinone (701285-29-2)

Guidance literature:

In dichloromethane; at 20 ℃; for 6h;

DOI:10.1081/NCN-120027817

Reference yield: 88.0%

6-methyl-2-(2-hydroxyethyl)amino-8-(2-deoxy-3,5-di-O-p-toluoyl-β-D-ribofuranosyl)-O4-[2-(4-nitrophenyl)ethyl]-7(8H)-pteridinone (701285-29-2) + 2-(4-nitrophenyl)ethoxycarbonyl chloride (88091-68-3) → 6-methyl-2-{2-[2-(4-nitrophenyl)ethoxycarbonyloxy]ethyl}amino-8-(2-deoxy-3,5-di-O-p-toluoyl-β-D-ribofuranosyl)-O4-[2-(4-nitrophenyl)ethyl]-7(8H)-pteridinone

Guidance literature:

With pyridine; at 40 ℃; for 30h;

DOI:10.1081/NCN-120027817

Reference yield: 71.0%

6-methyl-2-(2-hydroxyethyl)amino-8-(2-deoxy-3,5-di-O-p-toluoyl-β-D-ribofuranosyl)-O4-[2-(4-nitrophenyl)ethyl]-7(8H)-pteridinone (701285-29-2) → 6-methyl-2-(2-hydroxyethyl)amino-8-(2-deoxy-3,5-di-O-p-toluoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1,4-dioxane; acetonitrile;

DOI:10.1081/NCN-120027817

upstream raw materials:

ethanolamine

8-(2-deoxy-3,5-di-O-toluoyl-β-D-ribofuranosyl)-6-methyl-2-methylsulfonyl-4-[2-(4-nitrophenyl)ethoxy]-8H-pteridin-7-one

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