1-(Cyclopropylmethyl)-4-[(4-isopropoxyphenyl)methyl]-5-methyl-3-(6-O-propionyl-β-D-glucopyranosyloxy)-1H-pyrazole

Base Information

Chemical Name:1-(Cyclopropylmethyl)-4-[(4-isopropoxyphenyl)methyl]-5-methyl-3-(6-O-propionyl-β-D-glucopyranosyloxy)-1H-pyrazole
CAS No.:454678-82-1
Molecular Formula:C₂₇H₃₈N₂O₈
Molecular Weight:518.607
Hs Code.:

Synonyms:1-(Cyclopropylmethyl)-4-[(4-isopropoxyphenyl)methyl]-5-methyl-3-(6-O-propionyl-β-D-glucopyranosyloxy)-1H-pyrazole

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Chemical Property of 1-(Cyclopropylmethyl)-4-[(4-isopropoxyphenyl)methyl]-5-methyl-3-(6-O-propionyl-β-D-glucopyranosyloxy)-1H-pyrazole

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Technology Process of 1-(Cyclopropylmethyl)-4-[(4-isopropoxyphenyl)methyl]-5-methyl-3-(6-O-propionyl-β-D-glucopyranosyloxy)-1H-pyrazole

There total 8 articles about 1-(Cyclopropylmethyl)-4-[(4-isopropoxyphenyl)methyl]-5-methyl-3-(6-O-propionyl-β-D-glucopyranosyloxy)-1H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 454678-80-9
1-(cyclopropylmethyl)-3-(β-D-glucopyranosyloxy)-4-[(4-isopropoxyphenyl)methyl]-5-methyl-1H-pyrazole

: 79-03-8
propionyl chloride

: 454678-82-1
1-(Cyclopropylmethyl)-4-[(4-isopropoxyphenyl)methyl]-5-methyl-3-(6-O-propionyl-β-D-glucopyranosyloxy)-1H-pyrazole

Guidance literature:: 1-(cyclopropylmethyl)-3-(β-D-glucopyranosyloxy)-4-[(4-isopropoxyphenyl)methyl]-5-methyl-1H-pyrazole; propionyl chloride; With 2,4,6-trimethyl-pyridine; at 0 ℃; for 3h;

With citric acid; In water;

Reference yield:

: 329044-14-6
1,2-dihydro-4-[(4-isopropoxyphenyl)methyl]-5-methyl-3H-pyrazol-3-one

: 454678-82-1
1-(Cyclopropylmethyl)-4-[(4-isopropoxyphenyl)methyl]-5-methyl-3-(6-O-propionyl-β-D-glucopyranosyloxy)-1H-pyrazole

Guidance literature:: Multi-step reaction with 4 steps

1: silver carbonate / tetrahydrofuran / 65 °C

2: sodium hydroxide / ethanol; water / 2 h / 20 °C

3: caesium carbonate / sodium iodide / DMF (N,N-dimethyl-formamide) / 72 h / 50 °C

4: 2,4,6-trimethyl-pyridine / 3 h / 0 °C

With 2,4,6-trimethyl-pyridine; sodium hydroxide; caesium carbonate; silver carbonate; sodium iodide; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); ethanol; water;

Reference yield:

: 329044-79-3
3-(β-D-glucopyranosyloxy)-4-[(4-isopropoxyphenyl)-methyl]-5-methyl-1H-pyrazole

: 454678-82-1
1-(Cyclopropylmethyl)-4-[(4-isopropoxyphenyl)methyl]-5-methyl-3-(6-O-propionyl-β-D-glucopyranosyloxy)-1H-pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / sodium iodide / DMF (N,N-dimethyl-formamide) / 72 h / 50 °C

2: 2,4,6-trimethyl-pyridine / 3 h / 0 °C

With 2,4,6-trimethyl-pyridine; caesium carbonate; sodium iodide; In DMF (N,N-dimethyl-formamide);