4-chlorobenzyl 4-[2-(1H-benzotriazol-5-ylcarbamoyl)ethyl-carbamoyl]piperazine-1-carboxylate

Base Information

Chemical Name:4-chlorobenzyl 4-[2-(1H-benzotriazol-5-ylcarbamoyl)ethyl-carbamoyl]piperazine-1-carboxylate
CAS No.:1246639-73-5
Molecular Formula:C₂₂H₂₄ClN₇O₄
Molecular Weight:485.93
Hs Code.:

Synonyms:4-chlorobenzyl 4-[2-(1H-benzotriazol-5-ylcarbamoyl)ethyl-carbamoyl]piperazine-1-carboxylate

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Chemical Property of 4-chlorobenzyl 4-[2-(1H-benzotriazol-5-ylcarbamoyl)ethyl-carbamoyl]piperazine-1-carboxylate

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Technology Process of 4-chlorobenzyl 4-[2-(1H-benzotriazol-5-ylcarbamoyl)ethyl-carbamoyl]piperazine-1-carboxylate

There total 3 articles about 4-chlorobenzyl 4-[2-(1H-benzotriazol-5-ylcarbamoyl)ethyl-carbamoyl]piperazine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 1144037-32-0
4-chlorobenzyl piperazine-1-carboxylate hydrochloride

: 1246640-02-7
C₉H₁₁N₅O*ClH

: 530-62-1
1,1'-carbonyldiimidazole

: 1246639-73-5
4-chlorobenzyl 4-[2-(1H-benzotriazol-5-ylcarbamoyl)ethyl-carbamoyl]piperazine-1-carboxylate

Guidance literature:: C₉H₁₁N₅O*ClH; 1,1'-carbonyldiimidazole; With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

4-chlorobenzyl piperazine-1-carboxylate hydrochloride; With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

Reference yield:

: 1246640-01-6
C₁₄H₁₉N₅O₃

: 1246639-73-5
4-chlorobenzyl 4-[2-(1H-benzotriazol-5-ylcarbamoyl)ethyl-carbamoyl]piperazine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; isopropyl alcohol / 1 h / 20 °C

2.1: triethylamine / N,N-dimethyl-formamide / 1 h / 20 °C

2.2: 2 h / 20 °C

With hydrogenchloride; triethylamine; isopropyl alcohol; In N,N-dimethyl-formamide;

Reference yield:

: 3325-11-9
5-aminobenzotriazole

: 1246639-73-5
4-chlorobenzyl 4-[2-(1H-benzotriazol-5-ylcarbamoyl)ethyl-carbamoyl]piperazine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16 h / 20 °C

2.1: hydrogenchloride; isopropyl alcohol / 1 h / 20 °C

3.1: triethylamine / N,N-dimethyl-formamide / 1 h / 20 °C

3.2: 2 h / 20 °C

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; isopropyl alcohol; In N,N-dimethyl-formamide;