1-phenyl-2,3,3a,3b,4,5,6,11b-octahydro-1H-dipyrrolo<1,2-a:3',2'-c>quinoline

Base Information

Chemical Name:1-phenyl-2,3,3a,3b,4,5,6,11b-octahydro-1H-dipyrrolo<1,2-a:3',2'-c>quinoline
CAS No.:54105-26-9
Molecular Formula:C₂₀H₂₂N₂
Molecular Weight:290.408
Hs Code.:

Synonyms:1-phenyl-2,3,3a,3b,4,5,6,11b-octahydro-1H-dipyrrolo<1,2-a:3',2'-c>quinoline

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Chemical Property of 1-phenyl-2,3,3a,3b,4,5,6,11b-octahydro-1H-dipyrrolo<1,2-a:3',2'-c>quinoline

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Technology Process of 1-phenyl-2,3,3a,3b,4,5,6,11b-octahydro-1H-dipyrrolo<1,2-a:3',2'-c>quinoline

There total 10 articles about 1-phenyl-2,3,3a,3b,4,5,6,11b-octahydro-1H-dipyrrolo<1,2-a:3',2'-c>quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 4641-57-0
1-phenylpyrrolidin-2-one

: 762-42-5
dimethyl acetylenedicarboxylate

: dimethyl 2-phenyl-2-azabicyclo[3.2.0]hept-6-ene-6,7-dicarboxylate

: 54105-26-9
1-phenyl-2,3,3a,3b,4,5,6,11b-octahydro-1H-dipyrrolo<1,2-a:3',2'-c>quinoline

Guidance literature:: 1-phenylpyrrolidin-2-one; With lithium triethylborohydride; In dichloromethane; at 0 ℃; for 0.0833333h;

dimethyl acetylenedicarboxylate; In dichloromethane; at 20 ℃; for 5h; Reagent/catalyst; Irradiation;
DOI:10.1002/anie.201710523

Reference yield: 35.0%

: 4096-21-3
N-phenylpyrrolidine

: 54105-26-9
1-phenyl-2,3,3a,3b,4,5,6,11b-octahydro-1H-dipyrrolo<1,2-a:3',2'-c>quinoline

Guidance literature:: With (1R,2R)-N₁,N₁-dipropylcyclohexane-1,2-diamine; trifluorormethanesulfonic acid; dichlorobis(dimethylgloximato)cobalt(IV); Ru⁽²⁺⁾*2Cl^(1-)*C₁₀H₈N₂*6H₂O; 3-nitrobenzoic acid; In acetonitrile; at -10 ℃; for 0.25h; diastereoselective reaction; Inert atmosphere; Irradiation;
DOI:10.1002/anie.201700572

Reference yield: 19.0%

: 4096-21-3
N-phenylpyrrolidine

: 635-90-5
1-phenylpyrrole

: 3-iodo-1-phenyl-1H-pyrrole

: 54105-26-9
1-phenyl-2,3,3a,3b,4,5,6,11b-octahydro-1H-dipyrrolo<1,2-a:3',2'-c>quinoline

Guidance literature:: With oxygen; copper diacetate; potassium iodide; In acetonitrile; at 80 ℃; for 12h; under 760.051 Torr;
DOI:10.1021/acs.orglett.7b04029