titanium isopropoxide phenylsilsesquioxane

Base Information

• Chemical Name: titanium isopropoxide phenylsilsesquioxane
• CAS No.: 723302-20-3
• Molecular Formula: C₄₅H₄₂O₁₃Si₇Ti
• Molecular Weight: 1035.3
• Mol file: 723302-20-3.mol

Synonyms:titanium isopropoxide phenylsilsesquioxane

Chemical Property of titanium isopropoxide phenylsilsesquioxane

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of titanium isopropoxide phenylsilsesquioxane

There total 2 articles about titanium isopropoxide phenylsilsesquioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

titanium(IV) isopropylate (546-68-9) + Phenyltrichlorosilane (98-13-5) → titanium isopropoxide phenylsilsesquioxane (723302-20-3)

Guidance literature:

With hydrogenchloride; water; In tetrahydrofuran; water or aq. HCl added to C6H5SiCl3 soln. in THF, shaked at 50°C for 18 h, centrifuged in vac., dissolved in THF, Ti(OCH(CH3)2)4 added, kept 5 h at 50°C, centrifuged in vac.; stored under Ar;

DOI:10.1002/1521-3773(20010216)40:4<740::AID-ANIE7400>3.0.CO;2-C

Reference yield:

titanium(IV) isopropylate (546-68-9) + 1,3,5,7,9,11,14-heptaphenyltricyclo[7.3.3.1(5,11)]heptasiloxane-endo-3,7,14-triol (444315-26-8) → titanium isopropoxide phenylsilsesquioxane (723302-20-3)

Guidance literature:

In tetrahydrofuran; mixed, heated at 60°C for 5 h; evapd.(vac.);

DOI:10.1016/S1381-1169(01)00494-0

upstream raw materials:

titanium(IV) isopropylate

Phenyltrichlorosilane

1,3,5,7,9,11,14-heptaphenyltricyclo[7.3.3.1(5,11)]heptasiloxane-endo-3,7,14-triol