15N₁-benzenediazonium tetrafluoroborate

Base Information

Chemical Name:15N₁-benzenediazonium tetrafluoroborate
CAS No.:56708-86-2
Molecular Formula:BF₄*C₆H₅N₂
Molecular Weight:192.917
Hs Code.:

15N<sub>1</sub>-benzenediazonium tetrafluoroborate

Synonyms:15N₁-benzenediazonium tetrafluoroborate

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Chemical Property of 15N₁-benzenediazonium tetrafluoroborate

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Technology Process of 15N₁-benzenediazonium tetrafluoroborate

There total 1 articles about 15N₁-benzenediazonium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7022-92-6
(15N)-aniline

: 7632-00-0
sodium nitrite

: 56708-86-2
15N₁-benzenediazonium tetrafluoroborate

Guidance literature:: In not given; react. of labeled arylamine and NaNO2;

Reference yield: 65.0%

: 56708-86-2
15N₁-benzenediazonium tetrafluoroborate

: 58694-74-9
[ReH₂(NO)(P(C₆H₅)3)3]

: 143-66-8
sodium tetraphenyl borate

: [ReH(NO)(C₆H₅⁽¹⁵⁾NNH)(PPh₃)3](BPh₄)

Guidance literature:: In dichloromethane; using Schlenk techniques; addn. of CH2Cl2 to equimolar amt. of ReH2(NO)(PPh3)3 and (Ph(15)NN)(BF4) at -196°C; stirring for 50 min at 0°C, removal of solvent under reduced pressure, treatment with EtOH, addn. of excess of NaBPh4; sepn. of solid; filtration, crystn. from CH2Cl2 and ethanol;
DOI:10.1016/S0022-328X(03)00589-8

Reference yield: 60.0%

: 56708-86-2
15N₁-benzenediazonium tetrafluoroborate

: 17185-29-4
RhH(CO)(P(C₆H₅)3)3

: 351228-20-1
[Rh(C₆H₅⁽¹⁵⁾NNH)(CO)(P(C₆H₅)3)3]⁽¹⁺⁾*BF₄^(1-)=[Rh(C₆H₅⁽¹⁵⁾NNH)(CO)(P(C₆H₅)3)3]BF₄

Guidance literature:: In dichloromethane; (inert atmosphere); addn. of CH2Cl2 to a mixt. of rhodium complex and diazonium salt at -196°C, warming to -5°C, stirring for 50 min; evapn., addn. of EtOH at -5°C, cooling to -25°C, filtration, drying in vac.;
DOI:10.1016/S0022-328X(01)00720-3