1,t-2-bis(3,4,5-trimethoxyphenyl)-c-3,c-4-bis(3,4-methylenedioxybenzoyl)-r-1,c-2-cyclobutanedinitrile

Base Information

• Chemical Name: 1,t-2-bis(3,4,5-trimethoxyphenyl)-c-3,c-4-bis(3,4-methylenedioxybenzoyl)-r-1,c-2-cyclobutanedinitrile
• CAS No.: 138037-38-4
• Molecular Formula: C₄₀H₃₄N₂O₁₂
• Molecular Weight: 734.716

Synonyms:1,t-2-bis(3,4,5-trimethoxyphenyl)-c-3,c-4-bis(3,4-methylenedioxybenzoyl)-r-1,c-2-cyclobutanedinitrile

Chemical Property of 1,t-2-bis(3,4,5-trimethoxyphenyl)-c-3,c-4-bis(3,4-methylenedioxybenzoyl)-r-1,c-2-cyclobutanedinitrile

Chemical Property:

Purity/Quality:

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Technology Process of 1,t-2-bis(3,4,5-trimethoxyphenyl)-c-3,c-4-bis(3,4-methylenedioxybenzoyl)-r-1,c-2-cyclobutanedinitrile

There total 9 articles about 1,t-2-bis(3,4,5-trimethoxyphenyl)-c-3,c-4-bis(3,4-methylenedioxybenzoyl)-r-1,c-2-cyclobutanedinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.8%

1,t-2-bis(3,4,5-trimethoxyphenyl)-c-3,c-4-bis(3,4-methylenedioxybenzoyl)-r-1,c-2-cyclobutanedinitrile (138037-38-4) → 1,t-2-bis(3,4,5-trimethoxyphenyl)-c-3,t-4-bis(3,4-methylenedioxybenzoyl)-r-1,c-2-cyclobutanedinitrile (138037-38-4,138127-80-7)

Guidance literature:

With silica gel; In dichloromethane; for 18h; Ambient temperature;

DOI:10.1016/S0040-4020(01)85506-X

Reference yield: 70.2%

(Z)-2-(3,4,5-trimethoxyphenyl)-4-(3,4-methylenedioxyphenyl)-4-oxo-2-butenonitrile (138037-37-3) → 1,t-2-bis(3,4,5-trimethoxyphenyl)-c-3,c-4-bis(3,4-methylenedioxybenzoyl)-r-1,c-2-cyclobutanedinitrile (138037-38-4)

Guidance literature:

In solid; for 4h; Irradiation;

DOI:10.1016/S0040-4020(01)85506-X

Reference yield: 27.7%

(E)-2-(3,4,5-trimethoxyphenyl)-4-(3,4-methylenedioxyphenyl)-4-oxo-2-butenonitrile (138037-36-2) → 1,t-2-bis(3,4,5-trimethoxyphenyl)-c-3,c-4-bis(3,4-methylenedioxybenzoyl)-r-1,c-2-cyclobutanedinitrile (138037-38-4) + 1,t-2-bis(3,4,5-trimethoxyphenyl)-c-3,t-4-bis(3,4-methylenedioxybenzoyl)-r-1,c-2-cyclobutanedinitrile (138037-38-4,138127-80-7) + (Z)-2-(3,4,5-trimethoxyphenyl)-4-(3,4-methylenedioxyphenyl)-4-oxo-2-butenonitrile (138037-37-3)

Guidance literature:

In solid; for 37.5h; Irradiation;

DOI:10.1248/cpb.39.2173 DOI:10.1016/S0040-4020(01)85506-X

upstream raw materials:

(E)-2-(3,4,5-trimethoxyphenyl)-4-(3,4-methylenedioxyphenyl)-4-oxo-2-butenonitrile

(Z)-2-(3,4,5-trimethoxyphenyl)-4-(3,4-methylenedioxyphenyl)-4-oxo-2-butenonitrile

4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)butyronitrile

Downstream raw materials:

1,t-2-bis(3,4,5-trimethoxyphenyl)-c-3,t-4-bis(3,4-methylenedioxybenzoyl)-r-1,c-2-cyclobutanedinitrile

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