2,3-methylenedioxy-9-(p-fluorobenzoyloxy)-10-methoxy-1,13-cycloprotoberberine chloride

Base Information

Chemical Name:2,3-methylenedioxy-9-(p-fluorobenzoyloxy)-10-methoxy-1,13-cycloprotoberberine chloride
CAS No.:1404305-79-8
Molecular Formula:C₂₈H₁₉FNO₅*Cl
Molecular Weight:503.914
Hs Code.:

Synonyms:2,3-methylenedioxy-9-(p-fluorobenzoyloxy)-10-methoxy-1,13-cycloprotoberberine chloride

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Chemical Property of 2,3-methylenedioxy-9-(p-fluorobenzoyloxy)-10-methoxy-1,13-cycloprotoberberine chloride

Chemical Property:

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Technology Process of 2,3-methylenedioxy-9-(p-fluorobenzoyloxy)-10-methoxy-1,13-cycloprotoberberine chloride

There total 5 articles about 2,3-methylenedioxy-9-(p-fluorobenzoyloxy)-10-methoxy-1,13-cycloprotoberberine chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1404305-70-9
2,3-methylenedioxy-9-hydroxy-10-methoxy-1,13-cycloprotoberberine chloride

: 403-43-0
4-fluorobenzoyl chloride

: 1404305-79-8
2,3-methylenedioxy-9-(p-fluorobenzoyloxy)-10-methoxy-1,13-cycloprotoberberine chloride

Guidance literature:: With pyridine; In acetonitrile; for 6h; Reflux;
DOI:10.1016/j.ejmech.2013.07.026

Reference yield:

: 483-15-8
7,8-dihydroberberine

: 1404305-79-8
2,3-methylenedioxy-9-(p-fluorobenzoyloxy)-10-methoxy-1,13-cycloprotoberberine chloride

Guidance literature:: Multi-step reaction with 4 steps

1: acetonitrile / 5 h / 85 - 95 °C

2: hydrogenchloride / water / 1 h / 20 °C

3: 0.5 h / 195 - 210 °C / 20 - 30 Torr

4: pyridine / acetonitrile / 6 h / Reflux

With pyridine; hydrogenchloride; In water; acetonitrile;
DOI:10.1016/j.ejmech.2013.07.026

Reference yield:

: 1404306-19-9
2,3-methylenedioxy-9,10-dimethoxy-1,13-cycloprotoberberine chloride

: 1404305-79-8
2,3-methylenedioxy-9-(p-fluorobenzoyloxy)-10-methoxy-1,13-cycloprotoberberine chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 0.5 h / 195 - 210 °C / 20 - 30 Torr

2: pyridine / acetonitrile / 6 h / Reflux

With pyridine; In acetonitrile;
DOI:10.1016/j.ejmech.2013.07.026