2,3-methylenedioxy-9,10-dimethoxy-1,13-cycloprotoberberine chloride

Base Information

Chemical Name:2,3-methylenedioxy-9,10-dimethoxy-1,13-cycloprotoberberine chloride
CAS No.:1404306-19-9
Molecular Formula:C₂₂H₁₈NO₄*Cl
Molecular Weight:395.842
Hs Code.:

Synonyms:2,3-methylenedioxy-9,10-dimethoxy-1,13-cycloprotoberberine chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-methylenedioxy-9,10-dimethoxy-1,13-cycloprotoberberine chloride

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Technology Process of 2,3-methylenedioxy-9,10-dimethoxy-1,13-cycloprotoberberine chloride

There total 1 articles about 2,3-methylenedioxy-9,10-dimethoxy-1,13-cycloprotoberberine chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 483-15-8
7,8-dihydroberberine

: 1404306-19-9
2,3-methylenedioxy-9,10-dimethoxy-1,13-cycloprotoberberine chloride

Guidance literature:: 7,8-dihydroberberine; With Glyoxal; acetic acid; In acetonitrile; at 95 ℃; for 6h;

With hydrogenchloride; In water;

Reference yield: 43.0%

: 1404306-19-9
2,3-methylenedioxy-9,10-dimethoxy-1,13-cycloprotoberberine chloride

: 100-58-3
phenylmagnesium bromide

: 1,2-methylenedioxy-7-phenyl-8,9-dimethoxycycloberberine bromide

Guidance literature:: 2,3-methylenedioxy-9,10-dimethoxy-1,13-cycloprotoberberine chloride; phenylmagnesium bromide; In tetrahydrofuran; at 0 - 60 ℃; for 3h; Inert atmosphere;

With bromine; acetic acid; at 60 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.ejmech.2019.02.058

Reference yield: 41.0%

: 1404306-19-9
2,3-methylenedioxy-9,10-dimethoxy-1,13-cycloprotoberberine chloride

: 352-13-6
4-flourophenylmagnesium bromide

: 1,2-methylenedioxy-7-(4-fluorophenyl)-8,9-dimethoxycycloberberine bromide

Guidance literature:: 2,3-methylenedioxy-9,10-dimethoxy-1,13-cycloprotoberberine chloride; 4-flourophenylmagnesium bromide; In tetrahydrofuran; at 0 - 60 ℃; for 3h; Inert atmosphere;

With bromine; acetic acid; at 60 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.ejmech.2019.02.058