Technology Process of C27H36O6
There total 7 articles about C27H36O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C20H30O6;
With
silver(l) oxide;
In
toluene;
at 20 ℃;
for 1h;
Inert atmosphere;
benzyl bromide;
In
toluene;
at 20 ℃;
for 4h;
Inert atmosphere;
Reflux;
DOI:10.1016/j.tetasy.2010.11.006
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: toluene-4-sulfonic acid / benzene / 0.5 h / 60 °C / Inert atmosphere
1.2: 1 h / 60 °C / Inert atmosphere
2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
3.1: methanol; potassium carbonate / 0.25 h / 0 °C / Inert atmosphere
4.1: silver(l) oxide / toluene / 1 h / 20 °C / Inert atmosphere
4.2: 4 h / 20 °C / Inert atmosphere; Reflux
With
methanol; di-isopropyl azodicarboxylate; potassium carbonate; toluene-4-sulfonic acid; triphenylphosphine; silver(l) oxide;
In
tetrahydrofuran; toluene; benzene;
2.1: Mitsunobu reaction;
DOI:10.1016/j.tetasy.2010.11.006
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: toluene-4-sulfonic acid / benzene / 0.5 h / 60 °C / Inert atmosphere
1.2: 1 h / 60 °C / Inert atmosphere
2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
3.1: methanol; potassium carbonate / 0.25 h / 0 °C / Inert atmosphere
4.1: silver(l) oxide / toluene / 1 h / 20 °C / Inert atmosphere
4.2: 4 h / 20 °C / Inert atmosphere; Reflux
With
methanol; di-isopropyl azodicarboxylate; potassium carbonate; toluene-4-sulfonic acid; triphenylphosphine; silver(l) oxide;
In
tetrahydrofuran; toluene; benzene;
2.1: Mitsunobu reaction;
DOI:10.1016/j.tetasy.2010.11.006