<(5-(Trifluoroethenyl)-1,3-phenylene)bis<2,2,2-trifluoro-1-(trifluoromethyl)ethylidene>oxy>bis

Base Information

Chemical Name:<(5-(Trifluoroethenyl)-1,3-phenylene)bis<2,2,2-trifluoro-1-(trifluoromethyl)ethylidene>oxy>bis
CAS No.:136365-60-1
Molecular Formula:C₂₀H₂₁F₁₅O₂Si₂
Molecular Weight:634.533
Hs Code.:

<(5-(Trifluoroethenyl)-1,3-phenylene)bis<2,2,2-trifluoro-1-(trifluoromethyl)ethylidene>oxy>bis<trimethylsilane>

Synonyms:<(5-(Trifluoroethenyl)-1,3-phenylene)bis<2,2,2-trifluoro-1-(trifluoromethyl)ethylidene>oxy>bis

Suppliers and Price of <(5-(Trifluoroethenyl)-1,3-phenylene)bis<2,2,2-trifluoro-1-(trifluoromethyl)ethylidene>oxy>bis

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Chemical Property of <(5-(Trifluoroethenyl)-1,3-phenylene)bis<2,2,2-trifluoro-1-(trifluoromethyl)ethylidene>oxy>bis

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Technology Process of <(5-(Trifluoroethenyl)-1,3-phenylene)bis<2,2,2-trifluoro-1-(trifluoromethyl)ethylidene>oxy>bis

There total 3 articles about <(5-(Trifluoroethenyl)-1,3-phenylene)bis<2,2,2-trifluoro-1-(trifluoromethyl)ethylidene>oxy>bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 105417-08-1
trifluoroethenylzinc bromide

: 136338-42-6
<(5-Iodo-1,3-phenylene)bis<2,2,2-trifluoro-1-(trifluoromethyl)ethylidene>oxy>bis

: 136365-60-1
<(5-(Trifluoroethenyl)-1,3-phenylene)bis<2,2,2-trifluoro-1-(trifluoromethyl)ethylidene>oxy>bis

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 50 ℃; for 21h;
DOI:10.1016/S0022-1139(00)80344-9

Reference yield:

: 53173-72-1
5-Iodo-α,α,α',α'-tetrakis(trifluoromethyl)-1,3-benzenedimethanol

: 136365-60-1
<(5-(Trifluoroethenyl)-1,3-phenylene)bis<2,2,2-trifluoro-1-(trifluoromethyl)ethylidene>oxy>bis

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / 64 h / 94 °C

2: 83 percent / tetrakis(triphenylphosphine)palladium / dimethylformamide / 21 h / 50 °C

tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide;
DOI:10.1016/S0022-1139(00)80344-9

Reference yield:

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 136365-60-1
<(5-(Trifluoroethenyl)-1,3-phenylene)bis<2,2,2-trifluoro-1-(trifluoromethyl)ethylidene>oxy>bis

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / 64 h / 94 °C

2: 83 percent / tetrakis(triphenylphosphine)palladium / dimethylformamide / 21 h / 50 °C

tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide;
DOI:10.1016/S0022-1139(00)80344-9