1-bromo-9-(4-methylbenzoyl)-5-[4-[2-(trimethylsilyl)ethoxycarbonyl]phenyl]dipyrromethane

Base Information

Chemical Name:1-bromo-9-(4-methylbenzoyl)-5-[4-[2-(trimethylsilyl)ethoxycarbonyl]phenyl]dipyrromethane
CAS No.:378750-97-1
Molecular Formula:C₂₉H₃₁BrN₂O₃Si
Molecular Weight:563.566
Hs Code.:

Synonyms:1-bromo-9-(4-methylbenzoyl)-5-[4-[2-(trimethylsilyl)ethoxycarbonyl]phenyl]dipyrromethane

Suppliers and Price of 1-bromo-9-(4-methylbenzoyl)-5-[4-[2-(trimethylsilyl)ethoxycarbonyl]phenyl]dipyrromethane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1-bromo-9-(4-methylbenzoyl)-5-[4-[2-(trimethylsilyl)ethoxycarbonyl]phenyl]dipyrromethane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of 1-bromo-9-(4-methylbenzoyl)-5-[4-[2-(trimethylsilyl)ethoxycarbonyl]phenyl]dipyrromethane

There total 3 articles about 1-bromo-9-(4-methylbenzoyl)-5-[4-[2-(trimethylsilyl)ethoxycarbonyl]phenyl]dipyrromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 378750-94-8
1-(4-methylbenzoyl)-5-[4-[2-(trimethylsilyl)ethoxycarbonyl]phenyl]dipyrromethane

: 378750-97-1
1-bromo-9-(4-methylbenzoyl)-5-[4-[2-(trimethylsilyl)ethoxycarbonyl]phenyl]dipyrromethane

Guidance literature:: With N-Bromosuccinimide; In tetrahydrofuran; at -78 ℃; for 1h;
DOI:10.1021/jo0104835

Reference yield:

: 74032-45-4
S-2-pyridyl 4-methylbenzothiolate

: 378750-97-1
1-bromo-9-(4-methylbenzoyl)-5-[4-[2-(trimethylsilyl)ethoxycarbonyl]phenyl]dipyrromethane

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / EtMgBr / tetrahydrofuran / 3 h / -78 °C

2: 81 percent / NBS / tetrahydrofuran / 1 h / -78 °C

With N-Bromosuccinimide; ethylmagnesium bromide; In tetrahydrofuran;
DOI:10.1021/jo0104835

Reference yield:

: 262267-30-1
5-[4-[2-(trimethylsilyl)ethoxycarbonyl]phenyl]dipyrromethane

: 378750-97-1
1-bromo-9-(4-methylbenzoyl)-5-[4-[2-(trimethylsilyl)ethoxycarbonyl]phenyl]dipyrromethane

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / EtMgBr / tetrahydrofuran / 3 h / -78 °C

2: 81 percent / NBS / tetrahydrofuran / 1 h / -78 °C

With N-Bromosuccinimide; ethylmagnesium bromide; In tetrahydrofuran;
DOI:10.1021/jo0104835