(2,4,6-trioxotetrahydropyrimidin-5(2H)-ylidene)diazenium

Base Information

• Chemical Name: (2,4,6-trioxotetrahydropyrimidin-5(2H)-ylidene)diazenium
• CAS No.: 31221-06-4
• Molecular Formula: C₄H₂N₄O₃
• Molecular Weight: 154.085
• Mol file: 31221-06-4.mol

Synonyms:Barbituricacid 5-diazo- (6CI,7CI); 5-Diazobarbituric acid; NSC 252062

Chemical Property of (2,4,6-trioxotetrahydropyrimidin-5(2H)-ylidene)diazenium

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: g/cm³

Purity/Quality:

99.9% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2,4,6-trioxotetrahydropyrimidin-5(2H)-ylidene)diazenium

There total 8 articles about (2,4,6-trioxotetrahydropyrimidin-5(2H)-ylidene)diazenium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.8%

BARBITURIC ACID (67-52-7,944357-77-1) → 5-diazo-pyrimidine-2,4,6-trione (31221-06-4,902267-12-3)

Guidance literature:

With 4-dodecylbenzenesulphonyl azide; triethylamine; In acetonitrile; Ambient temperature;

Reference yield:

sulfonamide + BARBITURIC ACID (67-52-7,944357-77-1) + azidoformamidinium hydrochloride + aminoguanidine bicarbonate (2582-30-1) → 5-diazo-pyrimidine-2,4,6-trione (31221-06-4,902267-12-3)

Guidance literature:

With hydrogenchloride; sodium nitrite; In water;

Reference yield:

→ 5-diazo-pyrimidine-2,4,6-trione (31221-06-4,902267-12-3)

Guidance literature:

With water;

upstream raw materials:

pyrimidinetetraone 5-hydrazone

5-sulfaminouracil

BARBITURIC ACID

5,5'-diazanediylidene-bis-pyrimidine-2,4,6-trione

Downstream raw materials:

uramil

5-(4-methoxyphenyl)barbituric acid

5-[4-(4-bromophenoxy)phenyl]barbituric acid

5-bromo-5-[4-(4-bromophenoxy)phenyl]pyrimidine-2,4,6-trione

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