2-methyl-N-(2-(3-methyl-3-(methyldisulfanyl)butan-2-ylamino)phenyl)-2-(methyldisulfanyl)propanamide

Base Information

• Chemical Name: 2-methyl-N-(2-(3-methyl-3-(methyldisulfanyl)butan-2-ylamino)phenyl)-2-(methyldisulfanyl)propanamide
• CAS No.: 1245574-65-5
• Molecular Formula: C₁₆H₂₄N₂O₂S₄
• Molecular Weight: 404.643

Synonyms:2-methyl-N-(2-(3-methyl-3-(methyldisulfanyl)butan-2-ylamino)phenyl)-2-(methyldisulfanyl)propanamide

Chemical Property of 2-methyl-N-(2-(3-methyl-3-(methyldisulfanyl)butan-2-ylamino)phenyl)-2-(methyldisulfanyl)propanamide

Chemical Property:

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Technology Process of 2-methyl-N-(2-(3-methyl-3-(methyldisulfanyl)butan-2-ylamino)phenyl)-2-(methyldisulfanyl)propanamide

There total 3 articles about 2-methyl-N-(2-(3-methyl-3-(methyldisulfanyl)butan-2-ylamino)phenyl)-2-(methyldisulfanyl)propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-mercapto-N-[2-(2-mercapto-2-methylpropionylamino)phenyl]-2-methylpropionamide (469867-87-6) + methanethiosulfonic acid S-methyl ester (2949-92-0,31761-75-8) → 2-methyl-N-(2-(3-methyl-3-(methyldisulfanyl)butan-2-ylamino)phenyl)-2-(methyldisulfanyl)propanamide (1245574-65-5)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2.5h;

DOI:10.1021/ic101148c

Reference yield: 50.0%

Dimethyldisulphide (624-92-0) + 2N(CH2CH3)4(1+)*FeCl(SC(CH3)2CONC6H4NCOC(CH3)2S)(2-)=(N(CH2CH3)4)2FeCl(SC(CH3)2CONC6H4NCOC(CH3)2S) → 7,7,10,10,19,19,22,22-octamethyl-5,12,17,24-tetrahydro-8,9,20,21-tetrathia-5,12,17,24-tetraaza-dibenzo[a,k]cycloeicosene-6,11,18,23-tetraone (933452-60-9) + 2-methyl-N-(2-(3-methyl-3-(methyldisulfanyl)butan-2-ylamino)phenyl)-2-(methyldisulfanyl)propanamide (1245574-65-5)

Guidance literature:

With iodine; In acetonitrile; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1021/ic101148c

Reference yield: 50.0%

Dimethyldisulphide (624-92-0) + N(CH2CH3)4(1+)*Cu(SC(CH3)2CONC6H4NCOC(CH3)2S)(1-)=N(CH2CH3)4Cu(SC(CH3)2CONC6H4NCOC(CH3)2S) → 7,7,10,10,19,19,22,22-octamethyl-5,12,17,24-tetrahydro-8,9,20,21-tetrathia-5,12,17,24-tetraaza-dibenzo[a,k]cycloeicosene-6,11,18,23-tetraone (933452-60-9) + 2-methyl-N-(2-(3-methyl-3-(methyldisulfanyl)butan-2-ylamino)phenyl)-2-(methyldisulfanyl)propanamide (1245574-65-5)

Guidance literature:

With iodine; In [D₃]acetonitrile; at 20 ℃; for 22h;

DOI:10.1021/ic101148c

upstream raw materials:

2-mercapto-N-[2-(2-mercapto-2-methylpropionylamino)phenyl]-2-methylpropionamide

methanethiosulfonic acid S-methyl ester

Dimethyldisulphide

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