[2,4,5,6,2',4',5',6'-2H₈]-enterolactone

Base Information

• Chemical Name: [2,4,5,6,2',4',5',6'-2H₈]-enterolactone
• CAS No.: 856412-16-3
• Molecular Formula: C₁₈H₁₈O₄
• Molecular Weight: 306.275
• Mol file: 856412-16-3.mol

Synonyms:[2,4,5,6,2',4',5',6'-2H₈]-enterolactone

Chemical Property of [2,4,5,6,2',4',5',6'-2H₈]-enterolactone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of [2,4,5,6,2',4',5',6'-2H₈]-enterolactone

There total 1 articles about [2,4,5,6,2',4',5',6'-2H₈]-enterolactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

(3R*,4R*)-3-(3-hydroxybenzyl)-4-(3-hydroxybenzyl)-4,5-dihydro-2(3H)-furanone <(+/-)-HPMF> (76543-15-2) → [2,4,5,6,2',4',5',6'-2H8]-enterolactone (856412-16-3)

Guidance literature:

(3R^*,4R^*)-3-(3-hydroxybenzyl)-4-(3-hydroxybenzyl)-4,5-dihydro-2(3H)-furanone <(+/-)-HPMF>; With water-d2; In acetone;

With boron trifluoride - phosphoric-2H₃ acid; water-d2; at 20 ℃; for 20h;

DOI:10.1002/jlcr.793

Reference yield:

[2,4,5,6,2',4',5',6'-2H8]-enterolactone (856412-16-3) + chloro-trimethyl-silane (75-77-4) → C24H26(2)H8O4Si2

Guidance literature:

With pyridine; 1,1,1,3,3,3-hexamethyl-disilazane; for 2h;

DOI:10.1002/jlcr.793

upstream raw materials:

(3R^*,4R^*)-3-(3-hydroxybenzyl)-4-(3-hydroxybenzyl)-4,5-dihydro-2(3H)-furanone <(+/-)-HPMF>