4-{[4-(1-methyl-1H-pyrazol-5-yl)phenyl]sulfanyl}furo[3,2-c]pyridine trifluoroacetate salt

Base Information

Chemical Name:4-{[4-(1-methyl-1H-pyrazol-5-yl)phenyl]sulfanyl}furo[3,2-c]pyridine trifluoroacetate salt
CAS No.:1609577-18-5
Molecular Formula:C₂HF₃O₂*C₁₇H₁₃N₃OS
Molecular Weight:421.4
Hs Code.:

Synonyms:4-{[4-(1-methyl-1H-pyrazol-5-yl)phenyl]sulfanyl}furo[3,2-c]pyridine trifluoroacetate salt

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Chemical Property of 4-{[4-(1-methyl-1H-pyrazol-5-yl)phenyl]sulfanyl}furo[3,2-c]pyridine trifluoroacetate salt

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Technology Process of 4-{[4-(1-methyl-1H-pyrazol-5-yl)phenyl]sulfanyl}furo[3,2-c]pyridine trifluoroacetate salt

There total 2 articles about 4-{[4-(1-methyl-1H-pyrazol-5-yl)phenyl]sulfanyl}furo[3,2-c]pyridine trifluoroacetate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

: 1609581-10-3
4-[(4-bromophenyl)sulfanyl]furo[3,2-c]pyridine

: 76-05-1
trifluoroacetic acid

: 720702-41-0
(1-methyl-1H-pyrazol-5-yl)boronic acid

: 1609577-18-5
4-{[4-(1-methyl-1H-pyrazol-5-yl)phenyl]sulfanyl}furo[3,2-c]pyridine trifluoroacetate salt

Guidance literature:: 4-[(4-bromophenyl)sulfanyl]furo[3,2-c]pyridine; (1-methyl-1H-pyrazol-5-yl)boronic acid; With palladium diacetate; potassium carbonate; triphenylphosphine; In water; N,N-dimethyl-formamide; at 80 ℃; for 18h; Inert atmosphere;

trifluoroacetic acid; In water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 106-53-6
para-bromobenzenethiol

: 31270-80-1
4-chlorofuro[3,2-c]pyridine

: 1609577-18-5
4-{[4-(1-methyl-1H-pyrazol-5-yl)phenyl]sulfanyl}furo[3,2-c]pyridine trifluoroacetate salt

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / dimethyl sulfoxide / 16 h / 80 °C

2: triphenylphosphine; potassium carbonate; palladium diacetate / water; N,N-dimethyl-formamide / 18 h / 80 °C / Inert atmosphere

With palladium diacetate; potassium carbonate; caesium carbonate; triphenylphosphine; In water; dimethyl sulfoxide; N,N-dimethyl-formamide;